5,5'-Diphenyl-[2,2']bi[3,4-diaza-bicyclo[4.1.0]heptyl]-2,4,2',4'-tetraene

Base Information

Chemical Name:5,5'-Diphenyl-[2,2']bi[3,4-diaza-bicyclo[4.1.0]heptyl]-2,4,2',4'-tetraene
CAS No.:159538-42-8
Molecular Formula:C₂₂H₁₈N₄
Molecular Weight:338.412
Hs Code.:

Synonyms:5,5'-Diphenyl-[2,2']bi[3,4-diaza-bicyclo[4.1.0]heptyl]-2,4,2',4'-tetraene

Suppliers and Price of 5,5'-Diphenyl-[2,2']bi[3,4-diaza-bicyclo[4.1.0]heptyl]-2,4,2',4'-tetraene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5,5'-Diphenyl-[2,2']bi[3,4-diaza-bicyclo[4.1.0]heptyl]-2,4,2',4'-tetraene

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Technology Process of 5,5'-Diphenyl-[2,2']bi[3,4-diaza-bicyclo[4.1.0]heptyl]-2,4,2',4'-tetraene

There total 4 articles about 5,5'-Diphenyl-[2,2']bi[3,4-diaza-bicyclo[4.1.0]heptyl]-2,4,2',4'-tetraene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 2781-85-3
cyclopropene

: 133636-03-0
6,6'-Diphenyl-[3,3']bi[[1,2,4,5]tetrazinyl]

: 159538-42-8
5,5'-Diphenyl-[2,2']bi[3,4-diaza-bicyclo[4.1.0]heptyl]-2,4,2',4'-tetraene

Guidance literature:: In dichloromethane;
DOI:10.1016/0040-4039(94)80015-4

Reference yield:

: 35658-16-3
Oxalsaeure-bis-<β-benzoylhydrazid>

: 159538-42-8
5,5'-Diphenyl-[2,2']bi[3,4-diaza-bicyclo[4.1.0]heptyl]-2,4,2',4'-tetraene

Guidance literature:: Multi-step reaction with 4 steps

1: 5 percent / PCl₅ / 140 °C

2: 73 percent / 100percent N₂H₄ / ethanol / 0.17 h / 70 °C

3: NO_x / CH₂Cl₂

4: 81 percent / CH₂Cl₂

With NO_x; phosphorus pentachloride; hydrazine; In ethanol; dichloromethane;
DOI:10.1016/0040-4039(94)80015-4

Reference yield:

: C₁₆H₁₀Cl₄N₄

: 159538-42-8
5,5'-Diphenyl-[2,2']bi[3,4-diaza-bicyclo[4.1.0]heptyl]-2,4,2',4'-tetraene

Guidance literature:: Multi-step reaction with 3 steps

1: 73 percent / 100percent N₂H₄ / ethanol / 0.17 h / 70 °C

2: NO_x / CH₂Cl₂

3: 81 percent / CH₂Cl₂

With NO_x; hydrazine; In ethanol; dichloromethane;
DOI:10.1016/0040-4039(94)80015-4