N-(3-(aminomethyl)benzyl)-3,5-dichloro-N-(4-fluorobenzyl)-2-hydroxybenzenesulfonamide trifluoroacetate

Base Information

Chemical Name:N-(3-(aminomethyl)benzyl)-3,5-dichloro-N-(4-fluorobenzyl)-2-hydroxybenzenesulfonamide trifluoroacetate
CAS No.:1201663-18-4
Molecular Formula:C₂HF₃O₂*C₂₁H₁₉Cl₂FN₂O₃S
Molecular Weight:583.388
Hs Code.:

Synonyms:N-(3-(aminomethyl)benzyl)-3,5-dichloro-N-(4-fluorobenzyl)-2-hydroxybenzenesulfonamide trifluoroacetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(3-(aminomethyl)benzyl)-3,5-dichloro-N-(4-fluorobenzyl)-2-hydroxybenzenesulfonamide trifluoroacetate

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Technology Process of N-(3-(aminomethyl)benzyl)-3,5-dichloro-N-(4-fluorobenzyl)-2-hydroxybenzenesulfonamide trifluoroacetate

There total 4 articles about N-(3-(aminomethyl)benzyl)-3,5-dichloro-N-(4-fluorobenzyl)-2-hydroxybenzenesulfonamide trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1201660-71-0
tert-butyl 3-((3,5-dichloro-N-(4-fluorobenzyl)-2-hydroxyphenylsulfonamido)methyl)benzylcarbamate

: 76-05-1
trifluoroacetic acid

: 1201663-18-4
N-(3-(aminomethyl)benzyl)-3,5-dichloro-N-(4-fluorobenzyl)-2-hydroxybenzenesulfonamide trifluoroacetate

Guidance literature:: In dichloromethane; at 20 ℃; for 2.5h;

Reference yield:

: 108467-99-8
1-(N-Boc-aminomethyl)-3-(aminomethyl)benzene

: 1201663-18-4
N-(3-(aminomethyl)benzyl)-3,5-dichloro-N-(4-fluorobenzyl)-2-hydroxybenzenesulfonamide trifluoroacetate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium tris(acetoxy)borohydride / methanol / 5 h / 20 °C

2: dichloromethane / 1.5 h / 20 °C

3: dichloromethane / 2.5 h / 20 °C

With sodium tris(acetoxy)borohydride; In methanol; dichloromethane;

Reference yield:

: 459-57-4
4-fluorobenzaldehyde

: 1201663-18-4
N-(3-(aminomethyl)benzyl)-3,5-dichloro-N-(4-fluorobenzyl)-2-hydroxybenzenesulfonamide trifluoroacetate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium tris(acetoxy)borohydride / methanol / 5 h / 20 °C

2: dichloromethane / 1.5 h / 20 °C

3: dichloromethane / 2.5 h / 20 °C

With sodium tris(acetoxy)borohydride; In methanol; dichloromethane;