4-((1S,2aS,8bS)-2,2-Dioxo-1-phenyl-2,2a,3,4-tetrahydro-1H-2λ⁶-thia-cyclobuta[a]naphthalen-8b-yl)-morpholine

Base Information

• Chemical Name: 4-((1S,2aS,8bS)-2,2-Dioxo-1-phenyl-2,2a,3,4-tetrahydro-1H-2λ⁶-thia-cyclobuta[a]naphthalen-8b-yl)-morpholine
• CAS No.: 123426-40-4
• Molecular Formula: C₂₁H₂₃NO₃S
• Molecular Weight: 369.485

Synonyms:4-((1S,2aS,8bS)-2,2-Dioxo-1-phenyl-2,2a,3,4-tetrahydro-1H-2λ⁶-thia-cyclobuta[a]naphthalen-8b-yl)-morpholine

Chemical Property of 4-((1S,2aS,8bS)-2,2-Dioxo-1-phenyl-2,2a,3,4-tetrahydro-1H-2λ⁶-thia-cyclobuta[a]naphthalen-8b-yl)-morpholine

Chemical Property:

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Safty Information:

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Technology Process of 4-((1S,2aS,8bS)-2,2-Dioxo-1-phenyl-2,2a,3,4-tetrahydro-1H-2λ⁶-thia-cyclobuta[a]naphthalen-8b-yl)-morpholine

There total 1 articles about 4-((1S,2aS,8bS)-2,2-Dioxo-1-phenyl-2,2a,3,4-tetrahydro-1H-2λ⁶-thia-cyclobuta[a]naphthalen-8b-yl)-morpholine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-(3,4-dihydro-1-naphthalenyl)morpholine (31401-28-2) + benzenesulfonyl chloride (1939-99-7) → 4-((1R,10S)-9,9-Dioxo-10-phenyl-9λ6-thia-tricyclo[6.2.2.02,7]dodeca-2,4,6-trien-1-yl)-morpholine (123426-43-7) + 4-((1S,2aS,8bS)-2,2-Dioxo-1-phenyl-2,2a,3,4-tetrahydro-1H-2λ6-thia-cyclobuta[a]naphthalen-8b-yl)-morpholine (123426-40-4)

Guidance literature:

With triethylamine; In benzene; at 0 ℃; for 5h; Yield given. Yields of byproduct given;

Reference yield: 100.0%

4-((1S,2aS,8bS)-2,2-Dioxo-1-phenyl-2,2a,3,4-tetrahydro-1H-2λ6-thia-cyclobuta[a]naphthalen-8b-yl)-morpholine (123426-40-4) → 2-Phenylmethanesulfonyl-3,4-dihydro-2H-naphthalen-1-one (123426-49-3)

Guidance literature:

With hydrogenchloride; In ethanol;

upstream raw materials:

4-(3,4-dihydro-1-naphthalenyl)morpholine

benzenesulfonyl chloride

Downstream raw materials:

2-Phenylmethanesulfonyl-3,4-dihydro-2H-naphthalen-1-one

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