C₅₇H₈₆O₆Si₃

Base Information

Chemical Name:C₅₇H₈₆O₆Si₃
CAS No.:1310025-40-1
Molecular Formula:C₅₇H₈₆O₆Si₃
Molecular Weight:951.563
Hs Code.:

C<sub>57</sub>H<sub>86</sub>O<sub>6</sub>Si<sub>3</sub>

Synonyms:C₅₇H₈₆O₆Si₃

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Chemical Property of C₅₇H₈₆O₆Si₃

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Technology Process of C₅₇H₈₆O₆Si₃

There total 8 articles about C₅₇H₈₆O₆Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1310025-39-8
C₆₀H₉₆O₇Si₄

: 1310025-40-1
C₅₇H₈₆O₆Si₃

Guidance literature:: With sodium hexamethyldisilazane; In tetrahydrofuran; for 0.675h; Inert atmosphere; Cooling with ice;
DOI:10.1021/ja203034k

Reference yield:

: 1310025-34-3
C₃₄H₄₄O₅Si

: 1310025-40-1
C₅₇H₈₆O₆Si₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium hexamethyldisilazane / tetrahydrofuran; N,N-dimethyl-formamide / 0.03 h / Inert atmosphere; Cooling with ice

1.2: 0.33 h / 0 °C / Inert atmosphere

2.1: n-butyllithium; diisopropylamine / tetrahydrofuran; pentane / 0.23 h / -78 - 0 °C / Inert atmosphere

2.2: 0.77 h / -78 °C / Inert atmosphere

2.3: -78 °C

3.1: pyridinium p-toluenesulfonate / 3 h / 45 °C / Inert atmosphere

4.1: sodium tetrahydroborate; ethanol / 15 h / -15 °C / Inert atmosphere

5.1: 1H-imidazole / dichloromethane / 2 h / 20 °C / Inert atmosphere

6.1: magnesium / diethyl ether / Inert atmosphere; Reflux

6.2: 1.22 h / -78 °C / Inert atmosphere

6.3: 70 h / 20 °C / Inert atmosphere

7.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.68 h / Inert atmosphere; Cooling with ice

With 1H-imidazole; sodium tetrahydroborate; n-butyllithium; ethanol; sodium hexamethyldisilazane; pyridinium p-toluenesulfonate; magnesium; diisopropylamine; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide; pentane;
DOI:10.1021/ja203034k

Reference yield:

: 1310025-36-5
C₄₇H₆₀O₈Si

: 1310025-40-1
C₅₇H₈₆O₆Si₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: pyridinium p-toluenesulfonate / 3 h / 45 °C / Inert atmosphere

2.1: sodium tetrahydroborate; ethanol / 15 h / -15 °C / Inert atmosphere

3.1: 1H-imidazole / dichloromethane / 2 h / 20 °C / Inert atmosphere

4.1: magnesium / diethyl ether / Inert atmosphere; Reflux

4.2: 1.22 h / -78 °C / Inert atmosphere

4.3: 70 h / 20 °C / Inert atmosphere

5.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.68 h / Inert atmosphere; Cooling with ice

With 1H-imidazole; sodium tetrahydroborate; ethanol; sodium hexamethyldisilazane; pyridinium p-toluenesulfonate; magnesium; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1021/ja203034k