2-cyano-N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)-4-nitrobenzenesulfonamide

Base Information

Chemical Name:2-cyano-N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)-4-nitrobenzenesulfonamide
CAS No.:1308255-86-8
Molecular Formula:C₁₄H₁₀BN₃O₆S
Molecular Weight:359.127
Hs Code.:

Synonyms:2-cyano-N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)-4-nitrobenzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-cyano-N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)-4-nitrobenzenesulfonamide

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Technology Process of 2-cyano-N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)-4-nitrobenzenesulfonamide

There total 3 articles about 2-cyano-N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)-4-nitrobenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.86%

: 1099632-44-6
2-cyano-4-nitrobenzenesulfonyl chloride

: 117098-94-9
(5-amino-2-hydroxymethylphenyl)boronic acid

: 1308255-86-8
2-cyano-N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)-4-nitrobenzenesulfonamide

Guidance literature:: With 4-methyl-morpholine; In acetonitrile; at 0 - 20 ℃; Product distribution / selectivity;

Reference yield:

: 16588-02-6
4-chloro-3-cyanonitrobenzene

: 1308255-86-8
2-cyano-N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)-4-nitrobenzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / acetonitrile / 20 °C

2: acetic acid; chlorine / water / 2 h / 15 °C

3: 4-methyl-morpholine / acetonitrile / 0 - 20 °C

With 4-methyl-morpholine; chlorine; potassium carbonate; acetic acid; In water; acetonitrile;

Reference yield:

: 175135-67-8
2-(benzylthio)-5-nitrobenzonitrile

: 1308255-86-8
2-cyano-N-(1-hydroxy-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)-4-nitrobenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid; chlorine / water / 2 h / 15 °C

2: 4-methyl-morpholine / acetonitrile / 0 - 20 °C

With 4-methyl-morpholine; chlorine; acetic acid; In water; acetonitrile;