3-(1,1,2,2-TETRAFLUOROETHOXY)BENZOIC ACID

Base Information

• Chemical Name: 3-(1,1,2,2-TETRAFLUOROETHOXY)BENZOIC ACID
• CAS No.: 70126-48-6
• Molecular Formula: C9H6F4O3
• Molecular Weight: 238.138
• Hs Code.: 29189900
• Mol file: 70126-48-6.mol

Synonyms:3-(1,1,2,2-Tetrafluoroethoxy)benzoicacid;3-(1,1,2,2-Tetrafluoro-ethoxy)-benzoic acid;

Chemical Property of 3-(1,1,2,2-TETRAFLUOROETHOXY)BENZOIC ACID

Chemical Property:

• Melting Point: 122-126 °C(lit.)
• Boiling Point: 288.4 °C at 760 mmHg
• Flash Point: 128.2 °C
• PSA: 46.53000
• Density: 1.446 g/cm³
• LogP: 2.62150

Purity/Quality:

99%, ^*data from raw suppliers

3-(1,1,2,2-Tetrafluoroethoxy)benzoic acid ^*data from reagent suppliers

Safty Information:

• Pictogram(s): C,Xi
• Hazard Codes: C,Xi
• Statements: 34
• Safety Statements: 26-36/37/39-45

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-(1,1,2,2-TETRAFLUOROETHOXY)BENZOIC ACID

There total 3 articles about 3-(1,1,2,2-TETRAFLUOROETHOXY)BENZOIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl 3-hydroxybenzoate (19438-10-9) → 3-(1',1',2',2'-tetrafluoroethoxy)-benzoic acid (70126-48-6)

Guidance literature:

Multi-step reaction with 2 steps

1: KOH / acetone / 45 - 52 °C

2: aq. KOH

With potassium hydroxide; In acetone;

DOI:10.2533/000942904777678226

Reference yield:

→ 3-(1',1',2',2'-tetrafluoroethoxy)-benzoic acid (70126-48-6)

Guidance literature:

<1,1,2,2-Tetrafluor-aethoxy>-m-tolyl-aether, wss. KMnO4, Siedetemp., 0.5d;

Reference yield:

3-(1,1,2,2-tetrafluoro-ethoxy)-benzoic acid methyl ester (70126-45-3) → 3-(1',1',2',2'-tetrafluoroethoxy)-benzoic acid (70126-48-6)

Guidance literature:

With potassium hydroxide;

DOI:10.2533/000942904777678226

upstream raw materials:

3-(1,1,2,2-tetrafluoro-ethoxy)-benzoic acid methyl ester

methyl 3-hydroxybenzoate

Downstream raw materials:

3-(1',1',2',2'-tetrafluoroethoxy)-benzoyl chloride

3-(1,1,2,2-tetrafluoro-ethoxy)-benzoic acid methyl ester

N-[3-({2-[(cyclopropylcarbonyl)amino]imidazo[1,2-b]pyridazin-6-yl}oxy)phenyl]-3-(1,1,2,2-tetrafluoroethoxy)benzamide

N-[3-({2-[(cyclopropylcarbonyl)amino]imidazo[1,2-b]pyridazin-6-yl}oxy)-4-methoxyphenyl]-3-(1,1,2,2-tetrafluoroethoxy)benzamide

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