(S)-(+)-3-methyl-1-phenylsulfonyl-2-butanol

Base Information

Chemical Name:(S)-(+)-3-methyl-1-phenylsulfonyl-2-butanol
CAS No.:296758-99-1
Molecular Formula:C₁₁H₁₆O₃S
Molecular Weight:228.312
Hs Code.:

Synonyms:(S)-(+)-3-methyl-1-phenylsulfonyl-2-butanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-(+)-3-methyl-1-phenylsulfonyl-2-butanol

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Technology Process of (S)-(+)-3-methyl-1-phenylsulfonyl-2-butanol

There total 4 articles about (S)-(+)-3-methyl-1-phenylsulfonyl-2-butanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 112683-61-1
3-methyl-1-(phenylsulfonyl)butan-2-one

: 296758-99-1
(S)-(+)-3-methyl-1-phenylsulfonyl-2-butanol

Guidance literature:: With phosphate buffer; D-glucose; Pichia minuta IAM 12215 strain; at 30 ℃; for 27.5h; pH=6.0;
DOI:10.1016/j.tetasy.2006.12.013

Reference yield:

: 90020-41-0
(1E)-3-methylbut-1-en-1-yl phenyl sulfone

: (R)-(-)-3-methyl-1-phenylsulfonyl-2-butanol

: 296758-99-1
(S)-(+)-3-methyl-1-phenylsulfonyl-2-butanol

Guidance literature:: (1E)-3-methylbut-1-en-1-yl phenyl sulfone; With methanol; (R)-(-)-1-[(S)-2-(diphenylphosphino)ferrocene]ethyldicyclohexylphosphine; bis(pinacol)diborane; copper(l) chloride; sodium t-butanolate; In tetrahydrofuran; at 20 ℃; Inert atmosphere;

With water; In tetrahydrofuran; at 20 ℃; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1039/c1cc11949d

Reference yield:

: 3112-85-4
methylphenylsulfonate

: 296758-99-1
(S)-(+)-3-methyl-1-phenylsulfonyl-2-butanol

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-BuLi / tetrahydrofuran; hexane / 1 h / -78 °C

1.2: 85 percent / tetrahydrofuran; hexane / 1 h / -78 °C

2.1: Trichosporon cutaneum IAM 12206 strain; glucose; phosphate buffer / 24 h / 30 °C / pH 6.0

With n-butyllithium; phosphate buffer; D-glucose; Trichosporon cutaneum IAM 12206 strain; In tetrahydrofuran; hexane;
DOI:10.1016/j.tetasy.2006.12.013