C₂₉H₄₅O₈P

Base Information

Chemical Name:C₂₉H₄₅O₈P
CAS No.:1400765-80-1
Molecular Formula:C₂₉H₄₅O₈P
Molecular Weight:552.645
Hs Code.:

C<sub>29</sub>H<sub>45</sub>O<sub>8</sub>P

Synonyms:C₂₉H₄₅O₈P

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Chemical Property of C₂₉H₄₅O₈P

Chemical Property:

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Technology Process of C₂₉H₄₅O₈P

There total 5 articles about C₂₉H₄₅O₈P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1400765-77-6
C₂₁H₂₈O₅

: 137348-86-8
di-tert-butyl diisopropylphosphoramide

: 1400765-80-1
C₂₉H₄₅O₈P

Guidance literature:: C₂₁H₂₈O₅; di-tert-butyl diisopropylphosphoramide; With 1H-imidazole; trifluoroacetic acid; In tetrahydrofuran; at 20 ℃; for 20h; Inert atmosphere;

With dihydrogen peroxide; In tetrahydrofuran; at 0 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/ja306596m

Reference yield:

: 1400765-75-4
C₁₅H₁₈O₃

: 1400765-80-1
C₂₉H₄₅O₈P

Guidance literature:: Multi-step reaction with 3 steps

1.1: diisopropyl-carbodiimide; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 48 h / 20 °C / Darkness; Inert atmosphere

2.1: toluene-4-sulfonic acid / methanol; dichloromethane / 3.5 h / 20 °C

3.1: 1H-imidazole; trifluoroacetic acid / tetrahydrofuran / 20 h / 20 °C / Inert atmosphere

3.2: 0.5 h / 0 °C / Inert atmosphere

With 1H-imidazole; benzotriazol-1-ol; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; diisopropyl-carbodiimide; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/ja306596m

Reference yield:

: 10602-04-7
(4-ethynylphenyl)methanol

: 1400765-80-1
C₂₉H₄₅O₈P

Guidance literature:: Multi-step reaction with 5 steps

1.1: diisopropyl-carbodiimide; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 16 h / 20 °C / Darkness; Inert atmosphere

2.1: toluene-4-sulfonic acid / methanol; dichloromethane / 2.5 h / 20 °C

3.1: diisopropyl-carbodiimide; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 48 h / 20 °C / Darkness; Inert atmosphere

4.1: toluene-4-sulfonic acid / methanol; dichloromethane / 3.5 h / 20 °C

5.1: 1H-imidazole; trifluoroacetic acid / tetrahydrofuran / 20 h / 20 °C / Inert atmosphere

5.2: 0.5 h / 0 °C / Inert atmosphere

With 1H-imidazole; benzotriazol-1-ol; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; diisopropyl-carbodiimide; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/ja306596m