Technology Process of C23H23ClO2
There total 8 articles about C23H23ClO2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium phosphate;
palladium diacetate; trisodium tris(3-sulfophenyl)phosphine;
In
water; acetonitrile;
at 160 ℃;
for 0.333333h;
Microwave irradiation;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sulfuric acid / water / Heating / reflux
1.2: 0.75 h / 0 - 5 °C
1.3: 20 - 80 °C
2.1: isopropylmagnesium chloride / tetrahydrofuran / 1.33 h / -78 - 20 °C
2.2: 2 h / -78 - 20 °C
3.1: mercury(II) diacetate / chloroform / 5 h / 40 °C
4.1: dmap / chloroform / 1.08 h / 20 - 80 °C
5.1: potassium phosphate / palladium diacetate; trisodium tris(3-sulfophenyl)phosphine / water; acetonitrile / 0.33 h / 160 °C / Microwave irradiation
With
dmap; potassium phosphate; sulfuric acid; mercury(II) diacetate; isopropylmagnesium chloride;
palladium diacetate; trisodium tris(3-sulfophenyl)phosphine;
In
tetrahydrofuran; chloroform; water; acetonitrile;
5.1: Suzuki-Miyaura reaction;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: isopropylmagnesium chloride / tetrahydrofuran / 1.33 h / -78 - 20 °C
1.2: 2 h / -78 - 20 °C
2.1: mercury(II) diacetate / chloroform / 5 h / 40 °C
3.1: dmap / chloroform / 1.08 h / 20 - 80 °C
4.1: potassium phosphate / palladium diacetate; trisodium tris(3-sulfophenyl)phosphine / water; acetonitrile / 0.33 h / 160 °C / Microwave irradiation
With
dmap; potassium phosphate; mercury(II) diacetate; isopropylmagnesium chloride;
palladium diacetate; trisodium tris(3-sulfophenyl)phosphine;
In
tetrahydrofuran; chloroform; water; acetonitrile;
4.1: Suzuki-Miyaura reaction;