3,5-bis-[3,5-bis-(2-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-benzyloxy]-benzoic acid methyl ester

Base Information

Chemical Name:3,5-bis-[3,5-bis-(2-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-benzyloxy]-benzoic acid methyl ester
CAS No.:720681-06-1
Molecular Formula:C₅₈H₉₂O₂₄
Molecular Weight:1173.35
Hs Code.:

Synonyms:3,5-bis-[3,5-bis-(2-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-benzyloxy]-benzoic acid methyl ester

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Chemical Property of 3,5-bis-[3,5-bis-(2-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-benzyloxy]-benzoic acid methyl ester

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Technology Process of 3,5-bis-[3,5-bis-(2-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-benzyloxy]-benzoic acid methyl ester

There total 6 articles about 3,5-bis-[3,5-bis-(2-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-benzyloxy]-benzoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 2150-44-9
1-carbomethoxy-3,5-dihydroxybenzene

: 499972-35-9
1-bromomethyl-3,5-bis-(2-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-benzene

: 720681-06-1
3,5-bis-[3,5-bis-(2-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-benzyloxy]-benzoic acid methyl ester

Guidance literature:: With potassium carbonate; potassium iodide; In acetone; for 72h; Heating;

Reference yield:

: 111-77-3,95507-80-5
2-(2-methoxyethoxy)ethyl alcohol

: 720681-06-1
3,5-bis-[3,5-bis-(2-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-benzyloxy]-benzoic acid methyl ester

Guidance literature:: Multi-step reaction with 7 steps

1: 86 percent / SOCl₂; pyridine

2: 57 percent / Na

3: 83 percent / SOCl₂; pyridine

4: 74 percent / K₂CO₃; KI / acetone / 72 h / Heating

5: 74 percent / LiAlH₄ / tetrahydrofuran / 8 h / 20 °C

6: 75 percent / CBr₄; PPh₃ / tetrahydrofuran / 4 h / 20 °C

7: 78 percent / K₂CO₃; KI / acetone / 72 h / Heating

With pyridine; lithium aluminium tetrahydride; thionyl chloride; carbon tetrabromide; sodium; potassium carbonate; triphenylphosphine; potassium iodide; In tetrahydrofuran; acetone;

Reference yield:

: 23783-42-8,95507-80-5
tetraethylene glycol monomethyl ether

: 720681-06-1
3,5-bis-[3,5-bis-(2-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-benzyloxy]-benzoic acid methyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 83 percent / SOCl₂; pyridine

2: 74 percent / K₂CO₃; KI / acetone / 72 h / Heating

3: 74 percent / LiAlH₄ / tetrahydrofuran / 8 h / 20 °C

4: 75 percent / CBr₄; PPh₃ / tetrahydrofuran / 4 h / 20 °C

5: 78 percent / K₂CO₃; KI / acetone / 72 h / Heating

With pyridine; lithium aluminium tetrahydride; thionyl chloride; carbon tetrabromide; potassium carbonate; triphenylphosphine; potassium iodide; In tetrahydrofuran; acetone;