N⁶-Benzoyl-2'-O-(tert-butyldimethylsilyl)-5'-O-(4-methyltrityl)adenosyl-<3'-P-(2-chlorphenyl)>-5'>-N⁶-benzoyl-2'-O-(tert-butyldimethylsilyl)adenosin-3'-(2-chlorphenyl)(2-cyaaethyl)phosphat

Base Information

• Chemical Name: N⁶-Benzoyl-2'-O-(tert-butyldimethylsilyl)-5'-O-(4-methyltrityl)adenosyl-<3'-P-(2-chlorphenyl)>-5'>-N⁶-benzoyl-2'-O-(tert-butyldimethylsilyl)adenosin-3'-(2-chlorphenyl)(2-cyaaethyl)phosphat
• CAS No.: 89480-36-4
• Molecular Formula: C₈₁H₈₇Cl₂N₁₁O₁₆P₂Si₂
• Molecular Weight: 1659.67

Synonyms:N⁶-Benzoyl-2'-O-(tert-butyldimethylsilyl)-5'-O-(4-methyltrityl)adenosyl-<3'-P-(2-chlorphenyl)>-5'>-N⁶-benzoyl-2'-O-(tert-butyldimethylsilyl)adenosin-3'-(2-chlorphenyl)(2-cyaaethyl)phosphat

Chemical Property of N⁶-Benzoyl-2'-O-(tert-butyldimethylsilyl)-5'-O-(4-methyltrityl)adenosyl-<3'-P-(2-chlorphenyl)>-5'>-N⁶-benzoyl-2'-O-(tert-butyldimethylsilyl)adenosin-3'-(2-chlorphenyl)(2-cyaaethyl)phosphat

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Technology Process of N⁶-Benzoyl-2'-O-(tert-butyldimethylsilyl)-5'-O-(4-methyltrityl)adenosyl-<3'-P-(2-chlorphenyl)>-5'>-N⁶-benzoyl-2'-O-(tert-butyldimethylsilyl)adenosin-3'-(2-chlorphenyl)(2-cyaaethyl)phosphat

There total 1 articles about N⁶-Benzoyl-2'-O-(tert-butyldimethylsilyl)-5'-O-(4-methyltrityl)adenosyl-<3'-P-(2-chlorphenyl)>-5'>-N⁶-benzoyl-2'-O-(tert-butyldimethylsilyl)adenosin-3'-(2-chlorphenyl)(2-cyaaethyl)phosphat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

N6-Benzoyl-2'-O-(tert-butyldimethylsilyl)adenosin-3'-(o-chlorphenyl)(β-cyanethyl)phosphat (75074-02-1) + Triaethylammonium-6-benzoyl-2'-O-(tert-butyldimethylsilyl)-5'-O-(4-methoxytrityl)adenosin-3'-(2-chlorphenyl)phosphat> (75082-92-7) → N6-Benzoyl-2'-O-(tert-butyldimethylsilyl)-5'-O-(4-methyltrityl)adenosyl-<3'-P-(2-chlorphenyl)>-5'>-N6-benzoyl-2'-O-(tert-butyldimethylsilyl)adenosin-3'-(2-chlorphenyl)(2-cyaaethyl)phosphat (89480-36-4)

Guidance literature:

With TPS-NI; In pyridine; for 60h; Ambient temperature;

DOI:10.1002/hlca.19830660713

Reference yield: 96.0%

triethylamine (121-44-8) + N6-Benzoyl-2'-O-(tert-butyldimethylsilyl)-5'-O-(4-methyltrityl)adenosyl-<3'-P-(2-chlorphenyl)>-5'>-N6-benzoyl-2'-O-(tert-butyldimethylsilyl)adenosin-3'-(2-chlorphenyl)(2-cyaaethyl)phosphat (89480-36-4) → Triaethylammonium-6-benzoyl-2'-O-(tert-butyldimethylsilyl)-5'-O-(4-methoxytrityl)adenosyl-<3'-P-(2-chlorphenyl)>-5'>-N6-benzoyl-2'-O-(tert-butyldimethylsilyl)adenosin-3'-(2-chlorphenyl)phosphat>

Guidance literature:

In pyridine; water; for 1.5h; Ambient temperature;

DOI:10.1002/hlca.19830660713

Reference yield: 93.0%

N6-Benzoyl-2'-O-(tert-butyldimethylsilyl)-5'-O-(4-methyltrityl)adenosyl-<3'-P-(2-chlorphenyl)>-5'>-N6-benzoyl-2'-O-(tert-butyldimethylsilyl)adenosin-3'-(2-chlorphenyl)(2-cyaaethyl)phosphat (89480-36-4) → N6-Benzoyl-2'-O-(tert-butyldimethylsilyl)adenosyl-<3'-P-(2-chlorphenyl)>-5'>-N6-benzoyl-2'-O-(tert-butyldimethylsilyl)adenosin-3'-(2-chlorphenyl)(2-cyaaethyl)phosphat

Guidance literature:

With toluene-4-sulfonic acid; In methanol; dichloromethane; at -8 ℃; for 5h;

DOI:10.1002/hlca.19830660713

upstream raw materials:

N⁶-Benzoyl-2'-O-(tert-butyldimethylsilyl)adenosin-3'-(o-chlorphenyl)(β-cyanethyl)phosphat

Triaethylammonium-6-benzoyl-2'-O-(tert-butyldimethylsilyl)-5'-O-(4-methoxytrityl)adenosin-3'-(2-chlorphenyl)phosphat>

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