3-(2-butyn-1-yl)-N-[[2-(2-butyn-1-yl)phenyl]carbonimidoyl]-2-naphthalenamine

Base Information

Chemical Name:3-(2-butyn-1-yl)-N-[[2-(2-butyn-1-yl)phenyl]carbonimidoyl]-2-naphthalenamine
CAS No.:1445988-72-6
Molecular Formula:C₂₅H₂₀N₂
Molecular Weight:348.447
Hs Code.:

Synonyms:3-(2-butyn-1-yl)-N-[[2-(2-butyn-1-yl)phenyl]carbonimidoyl]-2-naphthalenamine

Suppliers and Price of 3-(2-butyn-1-yl)-N-[[2-(2-butyn-1-yl)phenyl]carbonimidoyl]-2-naphthalenamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3-(2-butyn-1-yl)-N-[[2-(2-butyn-1-yl)phenyl]carbonimidoyl]-2-naphthalenamine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-(2-butyn-1-yl)-N-[[2-(2-butyn-1-yl)phenyl]carbonimidoyl]-2-naphthalenamine

There total 7 articles about 3-(2-butyn-1-yl)-N-[[2-(2-butyn-1-yl)phenyl]carbonimidoyl]-2-naphthalenamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1445988-84-0
N-[3-(2-butyn-1-yl)-2-naphthalenyl]-N'-[2-(2-butyn-1-yl)phenyl]thiourea

: 1445988-72-6
3-(2-butyn-1-yl)-N-[[2-(2-butyn-1-yl)phenyl]carbonimidoyl]-2-naphthalenamine

Guidance literature:: With dmap; methanesulfonyl chloride; triethylamine; In dichloromethane; at 0 ℃;
DOI:10.1039/c3cc42792g

Reference yield:

: 3-azido-2-naphthalenecarboxaldehyde

: 1445988-72-6
3-(2-butyn-1-yl)-N-[[2-(2-butyn-1-yl)phenyl]carbonimidoyl]-2-naphthalenamine

Guidance literature:: Multi-step reaction with 5 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / -78 °C

1.2: 0.33 h / -78 °C

2.1: triethylsilane; trifluoroacetic acid / dichloromethane / 16 h / -5 °C

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.25 h / 0 °C

4.1: ethanol / 20 h / 20 °C

5.1: triethylamine; dmap; methanesulfonyl chloride / dichloromethane / 0 °C

With triethylsilane; dmap; lithium aluminium tetrahydride; n-butyllithium; methanesulfonyl chloride; triethylamine; trifluoroacetic acid; In tetrahydrofuran; ethanol; hexane; dichloromethane;
DOI:10.1039/c3cc42792g

Reference yield:

: 1445988-78-2
3-azido-α-(1-propyn-1-yl)-2-naphthalenemethanol

: 1445988-72-6
3-(2-butyn-1-yl)-N-[[2-(2-butyn-1-yl)phenyl]carbonimidoyl]-2-naphthalenamine

Guidance literature:: Multi-step reaction with 4 steps

1: triethylsilane; trifluoroacetic acid / dichloromethane / 16 h / -5 °C

2: lithium aluminium tetrahydride / tetrahydrofuran / 0.25 h / 0 °C

3: ethanol / 20 h / 20 °C

4: triethylamine; dmap; methanesulfonyl chloride / dichloromethane / 0 °C

With triethylsilane; dmap; lithium aluminium tetrahydride; methanesulfonyl chloride; triethylamine; trifluoroacetic acid; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1039/c3cc42792g