(2R,3R,4S,5S,6R)-2-{3'-[(allyloxy)methyl]-5',6'-dihydro-1',4'-dithiin-2'-yl}-3,4,5-tri(benzyloxy)-6-[(benzyloxy)methyl]tetrahydro-2H-2-pyranol

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Chemical Name:(2R,3R,4S,5S,6R)-2-{3'-[(allyloxy)methyl]-5',6'-dihydro-1',4'-dithiin-2'-yl}-3,4,5-tri(benzyloxy)-6-[(benzyloxy)methyl]tetrahydro-2H-2-pyranol
CAS No.:613649-17-5
Molecular Formula:C₄₂H₄₆O₇S₂
Molecular Weight:726.955
Hs Code.:

Synonyms:(2R,3R,4S,5S,6R)-2-{3'-[(allyloxy)methyl]-5',6'-dihydro-1',4'-dithiin-2'-yl}-3,4,5-tri(benzyloxy)-6-[(benzyloxy)methyl]tetrahydro-2H-2-pyranol

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Chemical Property of (2R,3R,4S,5S,6R)-2-{3'-[(allyloxy)methyl]-5',6'-dihydro-1',4'-dithiin-2'-yl}-3,4,5-tri(benzyloxy)-6-[(benzyloxy)methyl]tetrahydro-2H-2-pyranol

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Technology Process of (2R,3R,4S,5S,6R)-2-{3'-[(allyloxy)methyl]-5',6'-dihydro-1',4'-dithiin-2'-yl}-3,4,5-tri(benzyloxy)-6-[(benzyloxy)methyl]tetrahydro-2H-2-pyranol

There total 1 articles about (2R,3R,4S,5S,6R)-2-{3'-[(allyloxy)methyl]-5',6'-dihydro-1',4'-dithiin-2'-yl}-3,4,5-tri(benzyloxy)-6-[(benzyloxy)methyl]tetrahydro-2H-2-pyranol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 82598-84-3
2,3,4,6-tetra-O-benzyl-D-galactonolactone

: 5-[(allyloxy)methyl]-2,3-dihydro-1,4-dithiin

: 613649-17-5
(2R,3R,4S,5S,6R)-2-{3'-[(allyloxy)methyl]-5',6'-dihydro-1',4'-dithiin-2'-yl}-3,4,5-tri(benzyloxy)-6-[(benzyloxy)methyl]tetrahydro-2H-2-pyranol

Guidance literature:: With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 1.5h;
DOI:10.1016/S0008-6215(03)00275-1

Reference yield: 85.0%

: 613649-17-5
(2R,3R,4S,5S,6R)-2-{3'-[(allyloxy)methyl]-5',6'-dihydro-1',4'-dithiin-2'-yl}-3,4,5-tri(benzyloxy)-6-[(benzyloxy)methyl]tetrahydro-2H-2-pyranol

: 613649-18-6
(2R,3R,4S,5S,6R)-2-{3'-[(allyloxy)methyl]-5',6'-dihydro-1',4'-dithiin-2'-yl}-3,4,5-tri(benzyloxy)-6-[(benzyloxy)methyl]tetrahydro-2H-2-pyran

Guidance literature:: With triethylsilane; boron trifluoride diethyl etherate; In dichloromethane; acetonitrile; at -40 ℃; for 1.33333h;
DOI:10.1016/S0008-6215(03)00275-1