Trifluoro-methanesulfonic acid 2-((E)-6-methoxymethoxy-4-methyl-hex-4-enyl)-phenyl ester

Base Information

Chemical Name:Trifluoro-methanesulfonic acid 2-((E)-6-methoxymethoxy-4-methyl-hex-4-enyl)-phenyl ester
CAS No.:151950-85-5
Molecular Formula:C₁₆H₂₁F₃O₅S
Molecular Weight:382.401
Hs Code.:

Synonyms:Trifluoro-methanesulfonic acid 2-((E)-6-methoxymethoxy-4-methyl-hex-4-enyl)-phenyl ester

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Chemical Property of Trifluoro-methanesulfonic acid 2-((E)-6-methoxymethoxy-4-methyl-hex-4-enyl)-phenyl ester

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Technology Process of Trifluoro-methanesulfonic acid 2-((E)-6-methoxymethoxy-4-methyl-hex-4-enyl)-phenyl ester

There total 9 articles about Trifluoro-methanesulfonic acid 2-((E)-6-methoxymethoxy-4-methyl-hex-4-enyl)-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 151950-94-6
1-tert-butyldimethylsilyloxy-2-(2-propenyl)benzene

: 151950-85-5
Trifluoro-methanesulfonic acid 2-((E)-6-methoxymethoxy-4-methyl-hex-4-enyl)-phenyl ester

Guidance literature:: Multi-step reaction with 8 steps

1: OsO₄, NaIO₄, H₂O / tetrahydrofuran / 23 °C

2: benzene / 50 °C

3: H₂ / Pd/C / ethanol / 23 °C

4: NaH / tetrahydrofuran / 23 °C

5: Dibal-H / diethyl ether / -78 °C

6: 93 percent / i-Pr₂NEt / CH₂Cl₂ / 23 °C

7: tetrabutylammonium fluoride / tetrahydrofuran / 0 °C

8: Et₃N / CH₂Cl₂ / -78 - 0 °C

With sodium periodate; osmium(VIII) oxide; tetrabutyl ammonium fluoride; water; hydrogen; sodium hydride; diisobutylaluminium hydride; triethylamine; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane; benzene;
DOI:10.1021/ja00071a079

Reference yield:

: 939017-87-5
2-(2-((tert-butyldimethylsilyl)oxy)phenyl)acetaldehyde

: 151950-85-5
Trifluoro-methanesulfonic acid 2-((E)-6-methoxymethoxy-4-methyl-hex-4-enyl)-phenyl ester

Guidance literature:: Multi-step reaction with 7 steps

1: benzene / 50 °C

2: H₂ / Pd/C / ethanol / 23 °C

3: NaH / tetrahydrofuran / 23 °C

4: Dibal-H / diethyl ether / -78 °C

5: 93 percent / i-Pr₂NEt / CH₂Cl₂ / 23 °C

6: tetrabutylammonium fluoride / tetrahydrofuran / 0 °C

7: Et₃N / CH₂Cl₂ / -78 - 0 °C

With tetrabutyl ammonium fluoride; hydrogen; sodium hydride; diisobutylaluminium hydride; triethylamine; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane; benzene;
DOI:10.1021/ja00071a079

Reference yield:

: 151950-95-7
(E)-5-[2-(tert-Butyl-dimethyl-silanyloxy)-phenyl]-pent-3-en-2-one

: 151950-85-5
Trifluoro-methanesulfonic acid 2-((E)-6-methoxymethoxy-4-methyl-hex-4-enyl)-phenyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: H₂ / Pd/C / ethanol / 23 °C

2: NaH / tetrahydrofuran / 23 °C

3: Dibal-H / diethyl ether / -78 °C

4: 93 percent / i-Pr₂NEt / CH₂Cl₂ / 23 °C

5: tetrabutylammonium fluoride / tetrahydrofuran / 0 °C

6: Et₃N / CH₂Cl₂ / -78 - 0 °C

With tetrabutyl ammonium fluoride; hydrogen; sodium hydride; diisobutylaluminium hydride; triethylamine; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane;
DOI:10.1021/ja00071a079