(2S, 3S)-methyl 3-(4-fluorophenyl)-2-(diphenylmethyleneamino)-4-nitrobutanoate

Base Information

Chemical Name:(2S, 3S)-methyl 3-(4-fluorophenyl)-2-(diphenylmethyleneamino)-4-nitrobutanoate
CAS No.:1394134-00-9
Molecular Formula:C₂₄H₂₁FN₂O₄
Molecular Weight:420.44
Hs Code.:

Synonyms:(2S, 3S)-methyl 3-(4-fluorophenyl)-2-(diphenylmethyleneamino)-4-nitrobutanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S, 3S)-methyl 3-(4-fluorophenyl)-2-(diphenylmethyleneamino)-4-nitrobutanoate

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Technology Process of (2S, 3S)-methyl 3-(4-fluorophenyl)-2-(diphenylmethyleneamino)-4-nitrobutanoate

There total 2 articles about (2S, 3S)-methyl 3-(4-fluorophenyl)-2-(diphenylmethyleneamino)-4-nitrobutanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 706-08-1,5153-69-5
trans-1-(4-fluorophenyl)-2-nitro-ethene

: 81167-39-7
methyl N-(diphenylmethylene)glycinate

: 1394134-00-9
(2S, 3S)-methyl 3-(4-fluorophenyl)-2-(diphenylmethyleneamino)-4-nitrobutanoate

Guidance literature:: With C₃₆H₃₆FeN₃PS⁽²⁺⁾; silver(I) acetate; triethylamine; In tetrahydrofuran; at -25 ℃; for 3h; enantioselective reaction; Inert atmosphere;
DOI:10.1021/ol301916t

Reference yield: 67.0%

: 706-08-1,5153-69-5
trans-1-(4-fluorophenyl)-2-nitro-ethene

: 81477-94-3
N-(diphenylmethylene)glycine tert-butyl ester

: 1030830-50-2
(2S,3R,4S)-tert-butyl 3-(4-fuluorophenyl)-4-nitro-5,5-diphenylpyrrolidine-2-carboxylate

: 1394134-00-9
(2S, 3S)-methyl 3-(4-fluorophenyl)-2-(diphenylmethyleneamino)-4-nitrobutanoate

Guidance literature:: With C₃₆H₃₆FeN₃PS⁽²⁺⁾; silver(I) acetate; triethylamine; In tetrahydrofuran; at 20 ℃; for 24h; enantioselective reaction; Inert atmosphere;
DOI:10.1021/ol301916t