C₂₄H₃₆O₄

Base Information

Chemical Name:C₂₄H₃₆O₄
CAS No.:1312543-65-9
Molecular Formula:C₂₄H₃₆O₄
Molecular Weight:388.547
Hs Code.:

C<sub>24</sub>H<sub>36</sub>O<sub>4</sub>

Synonyms:C₂₄H₃₆O₄

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Chemical Property of C₂₄H₃₆O₄

Chemical Property:

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Technology Process of C₂₄H₃₆O₄

There total 10 articles about C₂₄H₃₆O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₀H₃₀O₃

: 1099-45-2
ethyl (triphenylphosphoranylidene)acetate

: 1312543-65-9
C₂₄H₃₆O₄

Guidance literature:: With benzoic acid; In toluene; at 90 ℃; for 0.25h;
DOI:10.1016/j.tetlet.2011.04.008

Reference yield:

: 910228-56-7
(2R)-2-[(4S,5S)-5-ethyl-2-(4-methoxyphenyl)-1,3-dioxan-4-yl]propan-1-ol

: 1312543-65-9
C₂₄H₃₆O₄

Guidance literature:: Multi-step reaction with 10 steps

1: 1H-imidazole; iodine; triphenylphosphine / tetrahydrofuran / 0.33 h / 50 °C

2: lithium chloride; lithium diisopropyl amide / tetrahydrofuran / 14 h / -78 - 20 °C

3: ammonia borane; lithium diisopropyl amide / tetrahydrofuran / 4 h / -78 - 20 °C

4: 2,6-dimethylpyridine / dichloromethane / 1 h / 0 - 20 °C

5: diisobutylaluminium hydride / dichloromethane / 2 h / -40 - -10 °C

6: sulfur trioxide pyridine complex / dichloromethane; dimethyl sulfoxide / 1.5 h / 0 - 20 °C

7: sodium hexamethyldisilazane / tetrahydrofuran / 18 h / -78 - 20 °C

8: tetrabutyl ammonium fluoride / tetrahydrofuran / 10 h / 0 - 20 °C

9: sulfur trioxide pyridine complex / dichloromethane; dimethyl sulfoxide / 1.5 h / 0 - 20 °C

10: benzoic acid / toluene / 0.25 h / 90 °C

With 1H-imidazole; 2,6-dimethylpyridine; ammonia borane; tetrabutyl ammonium fluoride; iodine; sodium hexamethyldisilazane; sulfur trioxide pyridine complex; diisobutylaluminium hydride; triphenylphosphine; benzoic acid; lithium chloride; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; toluene; 2: Myers alkylation reaction / 7: Wittig reaction / 10: Wittig reaction;
DOI:10.1016/j.tetlet.2011.04.008

Reference yield:

: 1312543-60-4
C₁₉H₃₀O₄

: 1312543-65-9
C₂₄H₃₆O₄

Guidance literature:: Multi-step reaction with 7 steps

1: 2,6-dimethylpyridine / dichloromethane / 1 h / 0 - 20 °C

2: diisobutylaluminium hydride / dichloromethane / 2 h / -40 - -10 °C

3: sulfur trioxide pyridine complex / dichloromethane; dimethyl sulfoxide / 1.5 h / 0 - 20 °C

4: sodium hexamethyldisilazane / tetrahydrofuran / 18 h / -78 - 20 °C

5: tetrabutyl ammonium fluoride / tetrahydrofuran / 10 h / 0 - 20 °C

6: sulfur trioxide pyridine complex / dichloromethane; dimethyl sulfoxide / 1.5 h / 0 - 20 °C

7: benzoic acid / toluene / 0.25 h / 90 °C

With 2,6-dimethylpyridine; tetrabutyl ammonium fluoride; sodium hexamethyldisilazane; sulfur trioxide pyridine complex; diisobutylaluminium hydride; benzoic acid; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; toluene; 4: Wittig reaction / 7: Wittig reaction;
DOI:10.1016/j.tetlet.2011.04.008