(N-tert-butoxycarbonyl)-3-(4-benzoylphenyl)-(S)-alaninyl-(S)-tyrosine methyl ester

Base Information

• Chemical Name: (N-tert-butoxycarbonyl)-3-(4-benzoylphenyl)-(S)-alaninyl-(S)-tyrosine methyl ester
• CAS No.: 1158565-02-6
• Molecular Formula: C₃₁H₃₄N₂O₇
• Molecular Weight: 546.62

Synonyms:(N-tert-butoxycarbonyl)-3-(4-benzoylphenyl)-(S)-alaninyl-(S)-tyrosine methyl ester

Chemical Property of (N-tert-butoxycarbonyl)-3-(4-benzoylphenyl)-(S)-alaninyl-(S)-tyrosine methyl ester

Chemical Property:

Purity/Quality:

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Technology Process of (N-tert-butoxycarbonyl)-3-(4-benzoylphenyl)-(S)-alaninyl-(S)-tyrosine methyl ester

There total 1 articles about (N-tert-butoxycarbonyl)-3-(4-benzoylphenyl)-(S)-alaninyl-(S)-tyrosine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

L-Tyr-OMe (1080-06-4) + N-tert-butoxycarbonyl-(R)-3-(4-benzoylphenyl)alanine → (N-tert-butoxycarbonyl)-3-(4-benzoylphenyl)-(S)-alaninyl-(S)-tyrosine methyl ester (1158565-02-6)

Guidance literature:

L-Tyr-OMe; N-tert-butoxycarbonyl-(R)-3-(4-benzoylphenyl)alanine; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 20 ℃; for 0.333333h;

With triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 20h;

DOI:10.1002/chem.200802674

Reference yield: 75.0%

(N-tert-butoxycarbonyl)-3-(4-benzoylphenyl)-(S)-alaninyl-(S)-tyrosine methyl ester (1158565-02-6) → c-(D)-bpa-(L)-Tyr (1280712-19-7)

Guidance literature:

(N-tert-butoxycarbonyl)-3-(4-benzoylphenyl)-(S)-alaninyl-(S)-tyrosine methyl ester; With formic acid; at 20 ℃; for 2h;

In toluene; iso-butanol; for 4h; Reflux;

DOI:10.1139/V10-110

upstream raw materials:

L-Tyr-OMe

Downstream raw materials:

c-(D)-bpa-(L)-Tyr

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