Technology Process of C70H79N4O20P
There total 10 articles about C70H79N4O20P which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium iodide;
In
acetone;
at 60 ℃;
for 96h;
DOI:10.1021/jo034471q
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 94 percent / NaBH4 / tetrahydrofuran; methanol / 0.83 h / 60 °C
2.1: 2,4,6-collidine / tetrahydrofuran / 4 h / 20 °C
2.2: 51 percent / I2 / tetrahydrofuran; H2O / 0.75 h / 20 °C
3.1: HCl / dioxane / 20 °C
4.1: 50 percent / Et3N / CH2Cl2 / 20 °C
5.1: 73 percent / NaI / acetone / 96 h / 60 °C
With
2,4,6-trimethyl-pyridine; hydrogenchloride; sodium tetrahydroborate; triethylamine; sodium iodide;
In
tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; acetone;
DOI:10.1021/jo034471q
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 70 percent / TiCl4 / CHCl3 / 19 h / 20 °C
2: 78 percent / sodium carbonate / acetonitrile / 19 h / Heating
3: 45 percent / H2NSO3H; NaClO2 / acetone; CHCl3; H2O / 20 °C
4: oxalyl chloride / CH2Cl2 / 6 h / 20 °C
5: 50 percent / Et3N / CH2Cl2 / 20 °C
6: 73 percent / NaI / acetone / 96 h / 60 °C
With
sodium chlorite; oxalyl dichloride; aminosulfonic acid; titanium tetrachloride; sodium carbonate; triethylamine; sodium iodide;
In
dichloromethane; chloroform; water; acetone; acetonitrile;
DOI:10.1021/jo034471q