N-(3,5-dimethyl-4-methoxyphenyl)-1-(4-methoxycarbonylphenyl)ethylideneamine

Base Information

Chemical Name:N-(3,5-dimethyl-4-methoxyphenyl)-1-(4-methoxycarbonylphenyl)ethylideneamine
CAS No.:948018-30-2
Molecular Formula:C₁₉H₂₁NO₃
Molecular Weight:311.381
Hs Code.:

Synonyms:N-(3,5-dimethyl-4-methoxyphenyl)-1-(4-methoxycarbonylphenyl)ethylideneamine

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Chemical Property of N-(3,5-dimethyl-4-methoxyphenyl)-1-(4-methoxycarbonylphenyl)ethylideneamine

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Technology Process of N-(3,5-dimethyl-4-methoxyphenyl)-1-(4-methoxycarbonylphenyl)ethylideneamine

There total 2 articles about N-(3,5-dimethyl-4-methoxyphenyl)-1-(4-methoxycarbonylphenyl)ethylideneamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 3609-53-8
methyl 4-acetylbenzoate

: 39785-37-0
4-amino-2,6-dimethylanisole

: 948018-30-2
N-(3,5-dimethyl-4-methoxyphenyl)-1-(4-methoxycarbonylphenyl)ethylideneamine

Guidance literature:: With 4 A molecular sieve; In toluene; Heating;
DOI:10.1021/ol071168t

Reference yield:

: 14804-39-8
2,6-dimethyl-4-nitroanisole

: 948018-30-2
N-(3,5-dimethyl-4-methoxyphenyl)-1-(4-methoxycarbonylphenyl)ethylideneamine

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / FeCl₃*6H₂O; NH₂NH₂*H₂O; charcoal / methanol / Heating

2: 75 percent / molecular sieves 4 Angstroem / toluene / Heating

With 4 A molecular sieve; iron(III) chloride; pyrographite; hydrazine hydrate; In methanol; toluene;
DOI:10.1021/ol071168t

Reference yield:

: 948018-30-2
N-(3,5-dimethyl-4-methoxyphenyl)-1-(4-methoxycarbonylphenyl)ethylideneamine

: (R)-N-(3,5-dimethyl-4-methoxyphenyl)-(1-(4-methoxycarbonylphenyl)ethyl)amine

: (S)-N-(3,5-dimethyl-4-methoxyphenyl)-(1-(4-methoxycarbonylphenyl)ethyl)amine

Guidance literature:: With hydrogen; (R_Fc)-1-Ph₂P-2-((S)-MeO(2-Py)CH)ferrocene iridium complex; In methanol; toluene; at 25 ℃; for 4h; under 7500.75 Torr; Title compound not separated from byproducts.;
DOI:10.1021/ol071168t