[5,10,15-tris(3,5-di-tert-butylphenyl)-20-(4-methoxycarbonylphenyl)porphyrinato]zinc(II)

Base Information

Chemical Name:[5,10,15-tris(3,5-di-tert-butylphenyl)-20-(4-methoxycarbonylphenyl)porphyrinato]zinc(II)
CAS No.:1188524-99-3
Molecular Formula:C₇₀H₇₈N₄O₂Zn
Molecular Weight:1072.8
Hs Code.:

Synonyms:[5,10,15-tris(3,5-di-tert-butylphenyl)-20-(4-methoxycarbonylphenyl)porphyrinato]zinc(II)

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Chemical Property of [5,10,15-tris(3,5-di-tert-butylphenyl)-20-(4-methoxycarbonylphenyl)porphyrinato]zinc(II)

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Technology Process of [5,10,15-tris(3,5-di-tert-butylphenyl)-20-(4-methoxycarbonylphenyl)porphyrinato]zinc(II)

There total 4 articles about [5,10,15-tris(3,5-di-tert-butylphenyl)-20-(4-methoxycarbonylphenyl)porphyrinato]zinc(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 5-(4-methoxycarbonylphenyl)-10,15,20-tris(3,5-di-tert-butylphenyl)porphyrin

: 1188524-99-3
[5,10,15-tris(3,5-di-tert-butylphenyl)-20-(4-methoxycarbonylphenyl)porphyrinato]zinc(II)

Guidance literature:: With zinc(II) acetate dihydrate;
DOI:10.1002/chem.201100502

Reference yield: 10.0%

: 109-97-7,30604-81-0
pyrrole

: 17610-00-3
3,5-Di-tert-butylbenzaldehyde

: 1571-08-0
methyl 4-formylbenzoate

: 116123-17-2
zinc(II) tetra(3,5-di-tert-butyl)phenylporphyrin

: 1188524-99-3
[5,10,15-tris(3,5-di-tert-butylphenyl)-20-(4-methoxycarbonylphenyl)porphyrinato]zinc(II)

Guidance literature:: pyrrole; 3,5-Di-tert-butylbenzaldehyde; methyl 4-formylbenzoate; With zinc diacetate; propionic acid; at 100 ℃; for 5h;

With pyridine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; for 1h; Reflux;
DOI:10.1016/j.tet.2009.06.037

Reference yield:

: 1571-08-0
methyl 4-formylbenzoate

: 1188524-99-3
[5,10,15-tris(3,5-di-tert-butylphenyl)-20-(4-methoxycarbonylphenyl)porphyrinato]zinc(II)

Guidance literature:: Multi-step reaction with 2 steps

1.1: boron trifluoride diethyl etherate / chloroform / 2 h / 20 °C / Inert atmosphere

1.2: 12 h / Darkness; Inert atmosphere

1.3: Inert atmosphere

2.1: zinc(II) acetate dihydrate

With boron trifluoride diethyl etherate; zinc(II) acetate dihydrate; In chloroform;
DOI:10.1002/chem.201100502