1-<4-methyl-2-methoxyphenyl>-2--2-thioxo-1-ethanone

Base Information

Chemical Name:1-<4-methyl-2-methoxyphenyl>-2--2-thioxo-1-ethanone
CAS No.:221354-65-0
Molecular Formula:C₁₄H₁₇NO₃S
Molecular Weight:279.36
Hs Code.:

1-<4-methyl-2-methoxyphenyl>-2-<tetrahydro-2H-1,4-oxazin-4-yl>-2-thioxo-1-ethanone

Synonyms:1-<4-methyl-2-methoxyphenyl>-2--2-thioxo-1-ethanone

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Chemical Property of 1-<4-methyl-2-methoxyphenyl>-2--2-thioxo-1-ethanone

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Technology Process of 1-<4-methyl-2-methoxyphenyl>-2--2-thioxo-1-ethanone

There total 4 articles about 1-<4-methyl-2-methoxyphenyl>-2--2-thioxo-1-ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 110-91-8,99108-56-2
morpholine

: 35633-35-3
2-methoxy-4-methylacetophenone

: 221354-43-4
2-<4-methyl-2-(methoxy)phenyl>-1-tetrahydro-2H-1,4-oxazin-4-yl-1-ethanthione

: 221354-65-0
1-<4-methyl-2-methoxyphenyl>-2--2-thioxo-1-ethanone

: 3,4-di-<4-methyl-2-methoxyphenyl>-thiophene

Guidance literature:: With sulfur; at 100 - 120 ℃; for 24h;
DOI:10.1016/S0040-4020(98)01096-5

Reference yield: 17.0%

: 110-91-8,99108-56-2
morpholine

: 35633-35-3
2-methoxy-4-methylacetophenone

: 221354-43-4
2-<4-methyl-2-(methoxy)phenyl>-1-tetrahydro-2H-1,4-oxazin-4-yl-1-ethanthione

: 221354-65-0
1-<4-methyl-2-methoxyphenyl>-2--2-thioxo-1-ethanone

: 2,5-bis-(2-methoxy-4-methyl-phenyl)-thiophene

Guidance literature:: With sulfur; at 100 ℃;
DOI:10.1016/S0040-4020(00)01055-3

Reference yield:

: 122-46-3
3-acetoxytoluene

: 221354-65-0
1-<4-methyl-2-methoxyphenyl>-2--2-thioxo-1-ethanone

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / ZrCl₄ / CH₂Cl₂ / 24 h / ultrasonic irradiation

2: 97 percent / potassium hydroxide / acetone / 15 h / Ambient temperature

3: 10 percent / S₈ / 24 h / 100 - 120 °C

With sulfur; potassium hydroxide; zirconium(IV) chloride; In dichloromethane; acetone;
DOI:10.1016/S0040-4020(98)01096-5