N-(5-phenyl-3H-1,2-dithiol-3-ylidene)propanthioamide

Base Information

• Chemical Name: N-(5-phenyl-3H-1,2-dithiol-3-ylidene)propanthioamide
• CAS No.: 930111-76-5
• Molecular Formula: C₁₂H₁₁NS₃
• Molecular Weight: 265.424
• Mol file: 930111-76-5.mol

Synonyms:N-(5-phenyl-3H-1,2-dithiol-3-ylidene)propanthioamide

Chemical Property of N-(5-phenyl-3H-1,2-dithiol-3-ylidene)propanthioamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-(5-phenyl-3H-1,2-dithiol-3-ylidene)propanthioamide

There total 1 articles about N-(5-phenyl-3H-1,2-dithiol-3-ylidene)propanthioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

(Z)-5-methyl-2-(2-oxo-2-phenylethylidene)thiazolidin-4-one → N-(5-phenyl-3H-1,2-dithiol-3-ylidene)propanamide (930111-77-6) + N-(5-phenyl-3H-1,2-dithiol-3-ylidene)propanthioamide (930111-76-5)

Guidance literature:

With Lawessons reagent; In toluene; Heating;

DOI:10.1016/j.tet.2006.12.075

Reference yield: 60.0%

N-(5-phenyl-3H-1,2-dithiol-3-ylidene)propanthioamide (930111-76-5) → 2-ethyl-6-phenyl-2,3-dihydro-4H-1,3-thiazine-4-thione

Guidance literature:

N-(5-phenyl-3H-1,2-dithiol-3-ylidene)propanthioamide; With sodium tetrahydroborate; In ethanol; Heating;

With water; for 0.166667h;

DOI:10.1016/j.tet.2006.12.075

Reference yield: 52.0%

N-(5-phenyl-3H-1,2-dithiol-3-ylidene)propanthioamide (930111-76-5) → N-(5-phenyl-3H-1,2-dithiol-3-ylidene)propanamide (930111-77-6)

Guidance literature:

With mercury(II) diacetate; acetic acid; for 2.5h; Heating;

DOI:10.1016/j.tet.2006.12.075

Downstream raw materials:

N-(5-phenyl-3H-1,2-dithiol-3-ylidene)propanamide