2-carbomethoxyphenyl 1-neopentyl-2-tert-butyl-4-nitro-5-imidazolyl sulfone

Base Information

Chemical Name:2-carbomethoxyphenyl 1-neopentyl-2-tert-butyl-4-nitro-5-imidazolyl sulfone
CAS No.:135217-08-2
Molecular Formula:C₂₀H₂₇N₃O₆S
Molecular Weight:437.517
Hs Code.:

Synonyms:2-carbomethoxyphenyl 1-neopentyl-2-tert-butyl-4-nitro-5-imidazolyl sulfone

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Chemical Property of 2-carbomethoxyphenyl 1-neopentyl-2-tert-butyl-4-nitro-5-imidazolyl sulfone

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Technology Process of 2-carbomethoxyphenyl 1-neopentyl-2-tert-butyl-4-nitro-5-imidazolyl sulfone

There total 5 articles about 2-carbomethoxyphenyl 1-neopentyl-2-tert-butyl-4-nitro-5-imidazolyl sulfone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 135217-05-9
1-neopentyl-2-tert-butyl-4-nitro-5-imidazolyl 2-carbomethoxyphenyl sulfide

: 135217-08-2
2-carbomethoxyphenyl 1-neopentyl-2-tert-butyl-4-nitro-5-imidazolyl sulfone

Guidance literature:: With dihydrogen peroxide; In acetic acid; a) 60 deg C, 1.25 h, b) 70 deg C, 1.5 h, c) 80 deg C, 1.25 h;
DOI:10.1002/jhet.5570280307

Reference yield:

: 67867-46-3
N,N'-dineopentyloxamide

: 135217-08-2
2-carbomethoxyphenyl 1-neopentyl-2-tert-butyl-4-nitro-5-imidazolyl sulfone

Guidance literature:: Multi-step reaction with 4 steps

1: 36 percent / PCl₅ / 13.5 h / Heating

2: 1) conc. HNO₃, 2) conc. H₂SO₄ / 1) H₂O, 70 deg C, 0.5 h, 2) 2 h, reflux

3: 93 percent / NH₃ / ethanol / a) 50 deg C, b) room temp., 2 h

4: 83 percent / 30percent aq. H₂O₂ / acetic acid / a) 60 deg C, 1.25 h, b) 70 deg C, 1.5 h, c) 80 deg C, 1.25 h

With phosphorus pentachloride; sulfuric acid; ammonia; dihydrogen peroxide; nitric acid; In ethanol; acetic acid;
DOI:10.1002/jhet.5570280307

Reference yield:

: 5813-64-9
2.2-dimethylpropylamine

: 135217-08-2
2-carbomethoxyphenyl 1-neopentyl-2-tert-butyl-4-nitro-5-imidazolyl sulfone

Guidance literature:: Multi-step reaction with 5 steps

1: 91 percent / ethanol / 2 - 8 °C

2: 36 percent / PCl₅ / 13.5 h / Heating

3: 1) conc. HNO₃, 2) conc. H₂SO₄ / 1) H₂O, 70 deg C, 0.5 h, 2) 2 h, reflux

4: 93 percent / NH₃ / ethanol / a) 50 deg C, b) room temp., 2 h

5: 83 percent / 30percent aq. H₂O₂ / acetic acid / a) 60 deg C, 1.25 h, b) 70 deg C, 1.5 h, c) 80 deg C, 1.25 h

With phosphorus pentachloride; sulfuric acid; ammonia; dihydrogen peroxide; nitric acid; In ethanol; acetic acid;
DOI:10.1002/jhet.5570280307