Benzyl-6-O-acetyl-2-azido-3-O-<α,α-D2>benzyl-2-desoxy-4-O-(diphenoxyphosphoryl)-β-D-glucopyranosid

Base Information

Chemical Name:Benzyl-6-O-acetyl-2-azido-3-O-<α,α-D2>benzyl-2-desoxy-4-O-(diphenoxyphosphoryl)-β-D-glucopyranosid
CAS No.:106115-89-3
Molecular Formula:C₃₄H₃₄N₃O₉P
Molecular Weight:661.617
Hs Code.:

Synonyms:Benzyl-6-O-acetyl-2-azido-3-O-<α,α-D2>benzyl-2-desoxy-4-O-(diphenoxyphosphoryl)-β-D-glucopyranosid

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Chemical Property of Benzyl-6-O-acetyl-2-azido-3-O-<α,α-D2>benzyl-2-desoxy-4-O-(diphenoxyphosphoryl)-β-D-glucopyranosid

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Technology Process of Benzyl-6-O-acetyl-2-azido-3-O-<α,α-D2>benzyl-2-desoxy-4-O-(diphenoxyphosphoryl)-β-D-glucopyranosid

There total 2 articles about Benzyl-6-O-acetyl-2-azido-3-O-<α,α-D2>benzyl-2-desoxy-4-O-(diphenoxyphosphoryl)-β-D-glucopyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 106115-80-4
6-O-Acetyl-2-azido-3-O-<α,α-D2>benzyl-2-desoxy-4-O-(diphenoxyphosphoryl)-α-D-glucopyranosylbromid

: 100-51-6,185532-71-2
benzyl alcohol

: 106115-89-3
Benzyl-6-O-acetyl-2-azido-3-O-<α,α-D2>benzyl-2-desoxy-4-O-(diphenoxyphosphoryl)-β-D-glucopyranosid

Guidance literature:: With silver silicate; 4 A molecular sieve; In dichloromethane; at -20 ℃; for 3h;

Reference yield:

: 1,6-Di-O-acetyl-2-azido-3-O-<α,α-D2>benzyl-2-desoxy-4-O-(diphenoxyphosphoryl)-α,β-D-glucopyranose

: 106115-89-3
Benzyl-6-O-acetyl-2-azido-3-O-<α,α-D2>benzyl-2-desoxy-4-O-(diphenoxyphosphoryl)-β-D-glucopyranosid

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / TiBr₄ / CH₂Cl₂; ethyl acetate / 20 h / Ambient temperature

2: 96 percent / silver silicate, molecular sieve 4 Angstroem / CH₂Cl₂ / 3 h / -20 °C

With silver silicate; 4 A molecular sieve; titanium(IV) bromide; In dichloromethane; ethyl acetate;

Reference yield:

: 106115-89-3
Benzyl-6-O-acetyl-2-azido-3-O-<α,α-D2>benzyl-2-desoxy-4-O-(diphenoxyphosphoryl)-β-D-glucopyranosid

: 106115-90-6
Benzyl-6-O-acetyl-3-O-<α,α-D2>benzyl-2-desoxy-4-O-(diphenoxyphosphoryl)-2-(tetradecanoylamino)-β-D-glucopyranosid

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) H₂S, 2.) 0.5 N HCl / 1.) pyridine, H₂O, 4 h, 45 deg C, 2.) toluene, MeOH

2: 80 percent / pyridine / dioxane / 1 h / 0 °C

With pyridine; hydrogenchloride; hydrogen sulfide; In 1,4-dioxane;