trans-4-(3,3,3-trifluoropropanesulfonylmethyl)cyclohexane carbaldehyde

Base Information

Chemical Name:trans-4-(3,3,3-trifluoropropanesulfonylmethyl)cyclohexane carbaldehyde
CAS No.:1097630-06-2
Molecular Formula:C₁₁H₁₇F₃O₃S
Molecular Weight:286.315
Hs Code.:

Synonyms:trans-4-(3,3,3-trifluoropropanesulfonylmethyl)cyclohexane carbaldehyde

Suppliers and Price of trans-4-(3,3,3-trifluoropropanesulfonylmethyl)cyclohexane carbaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of trans-4-(3,3,3-trifluoropropanesulfonylmethyl)cyclohexane carbaldehyde

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of trans-4-(3,3,3-trifluoropropanesulfonylmethyl)cyclohexane carbaldehyde

There total 3 articles about trans-4-(3,3,3-trifluoropropanesulfonylmethyl)cyclohexane carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1097630-04-0
trans-4-(3,3,3-trifluoropropylsulfonylmethyl)cyclohexylmethanol

: 1097630-06-2
trans-4-(3,3,3-trifluoropropanesulfonylmethyl)cyclohexane carbaldehyde

Guidance literature:: trans-4-(3,3,3-trifluoropropylsulfonylmethyl)cyclohexylmethanol; With oxalyl dichloride; dimethyl sulfoxide; In dichloromethane; at -78 - -50 ℃; for 2h; Inert atmosphere;

With triethylamine; In dichloromethane; at -50 - 20 ℃; for 18.6667h; Inert atmosphere;

Reference yield:

: 109004-13-9
[4-(p-toluenesulfonyloxymethyl)cyclohexyl]methanol

: 1097630-06-2
trans-4-(3,3,3-trifluoropropanesulfonylmethyl)cyclohexane carbaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium thioacetate / dimethyl sulfoxide / 7 h / 20 - 60 °C

1.2: 1 h / 0 °C

1.3: 6 h / 60 °C

2.1: 3-chloro-benzenecarboperoxoic acid / chloroform / 4 h / 0 - 50 °C / Inert atmosphere

3.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 2 h / -78 - -50 °C / Inert atmosphere

3.2: 18.67 h / -50 - 20 °C / Inert atmosphere

With oxalyl dichloride; dimethyl sulfoxide; 3-chloro-benzenecarboperoxoic acid; potassium thioacetate; In dichloromethane; chloroform; dimethyl sulfoxide;

Reference yield:

: 1233934-87-6
4-(3,3,3-trifluoropropylthiomethyl)cyclohexanemethanol

: 1097630-06-2
trans-4-(3,3,3-trifluoropropanesulfonylmethyl)cyclohexane carbaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: 3-chloro-benzenecarboperoxoic acid / chloroform / 4 h / 0 - 50 °C / Inert atmosphere

2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 2 h / -78 - -50 °C / Inert atmosphere

2.2: 18.67 h / -50 - 20 °C / Inert atmosphere

With oxalyl dichloride; dimethyl sulfoxide; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; chloroform;