Technology Process of C51H45N7O6
There total 4 articles about C51H45N7O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
4-(prop-2-ynyloxy)benzoic acid;
With
diphenyl phosphoryl azide; triethylamine;
In
toluene;
at 25 - 70 ℃;
for 19h;
Inert atmosphere;
tris(m-aminobenzyl)amine;
at 70 ℃;
for 7h;
Inert atmosphere;
DOI:10.1039/c2cc33408a
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium carbonate / acetone / 18 h / 65 °C / Inert atmosphere
2.1: potassium hydroxide / ethanol; water / 16 h / 25 °C / Inert atmosphere
2.2: Inert atmosphere
3.1: diphenyl phosphoryl azide; triethylamine / toluene / 19 h / 25 - 70 °C / Inert atmosphere
3.2: 7 h / 70 °C / Inert atmosphere
With
diphenyl phosphoryl azide; potassium carbonate; triethylamine; potassium hydroxide;
In
ethanol; water; acetone; toluene;
DOI:10.1039/c2cc33408a
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: potassium hydroxide / ethanol; water / 16 h / 25 °C / Inert atmosphere
1.2: Inert atmosphere
2.1: diphenyl phosphoryl azide; triethylamine / toluene / 19 h / 25 - 70 °C / Inert atmosphere
2.2: 7 h / 70 °C / Inert atmosphere
With
diphenyl phosphoryl azide; triethylamine; potassium hydroxide;
In
ethanol; water; toluene;
DOI:10.1039/c2cc33408a
