N-[4-chloro-3-[[(tricyclo[3.3.1.1^3,7]dec-1-yImethyl)amino]carbonyl]benzoyl]-L-serine methyl ester

Base Information

• Chemical Name: N-[4-chloro-3-[[(tricyclo[3.3.1.1^3,7]dec-1-yImethyl)amino]carbonyl]benzoyl]-L-serine methyl ester
• CAS No.: 878206-69-0
• Molecular Formula: C₂₃H₂₉ClN₂O₅
• Molecular Weight: 448.947

Synonyms:N-[4-chloro-3-[[(tricyclo[3.3.1.1^3,7]dec-1-yImethyl)amino]carbonyl]benzoyl]-L-serine methyl ester

Chemical Property of N-[4-chloro-3-[[(tricyclo[3.3.1.1^3,7]dec-1-yImethyl)amino]carbonyl]benzoyl]-L-serine methyl ester

Chemical Property:

Purity/Quality:

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Technology Process of N-[4-chloro-3-[[(tricyclo[3.3.1.1^3,7]dec-1-yImethyl)amino]carbonyl]benzoyl]-L-serine methyl ester

There total 1 articles about N-[4-chloro-3-[[(tricyclo[3.3.1.1^3,7]dec-1-yImethyl)amino]carbonyl]benzoyl]-L-serine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-chloro-3-[[(tricyclo[3.3.1.13,7]dec-1-ylmethyl)amino]carbonyl]benzoic acid (878206-68-9) + methyl (2S)-2-amino-3-hydroxypropanoate hydrochloride (5680-80-8) → N-[4-chloro-3-[[(tricyclo[3.3.1.13,7]dec-1-yImethyl)amino]carbonyl]benzoyl]-L-serine methyl ester (878206-69-0)

Guidance literature:

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; at 0 - 20 ℃; for 16h;

Reference yield:

N-[4-chloro-3-[[(tricyclo[3.3.1.13,7]dec-1-yImethyl)amino]carbonyl]benzoyl]-L-serine methyl ester (878206-69-0) → 2-[4-chloro-3-[[(tricyclo[3.3.1.13,7]dec-1-ylmethyl)amino]carbonyl]phenyl]-4-oxazolecarboxylic acid methyl ester

Guidance literature:

N-[4-chloro-3-[[(tricyclo[3.3.1.1^3,7]dec-1-yImethyl)amino]carbonyl]benzoyl]-L-serine methyl ester; With diethylamino-sulfur trifluoride; In dichloromethane; at -78 - -30 ℃; for 1.16667h;

With sodium hydrogencarbonate; In dichloromethane; water; at -30 - 20 ℃;

With Bromotrichloromethane; 1,8-diazabicyclo[5.4.0]undec-7-ene; more than 3 stages;

upstream raw materials:

4-chloro-3-[[(tricyclo[3.3.1.1^3,7]dec-1-ylmethyl)amino]carbonyl]benzoic acid

methyl (2S)-2-amino-3-hydroxypropanoate hydrochloride

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