C₅₄H₈₁N₅O₁₂

Base Information

Chemical Name:C₅₄H₈₁N₅O₁₂
CAS No.:1610850-91-3
Molecular Formula:C₅₄H₈₁N₅O₁₂
Molecular Weight:992.263
Hs Code.:

C<sub>54</sub>H<sub>81</sub>N<sub>5</sub>O<sub>12</sub>

Synonyms:C₅₄H₈₁N₅O₁₂

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Chemical Property of C₅₄H₈₁N₅O₁₂

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Technology Process of C₅₄H₈₁N₅O₁₂

There total 24 articles about C₅₄H₈₁N₅O₁₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 1610850-88-8
C₆₀H₉₅N₅O₁₂Si

: 1610850-91-3
C₅₄H₈₁N₅O₁₂

Guidance literature:: With pyridine hydrogenfluoride; In tetrahydrofuran; at 0 ℃; for 2h;
DOI:10.1016/j.tetlet.2014.04.079

Reference yield:

: 1610850-49-1
(S)-methyl 2-((2S,3S)-2-(tert-butoxycarbonylamino)-N,3-dimethylpentanamido)propanoate

: 1610850-91-3
C₅₄H₈₁N₅O₁₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: dichloromethane / 2 h / 0 - 20 °C

2.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.17 h / 0 °C

2.2: 8 h / 20 °C

3.1: lithium hydroxide monohydrate / tetrahydrofuran; methanol; water / 1 h / 0 - 20 °C

4.1: triethylamine; dmap / dichloromethane / 4 h / 0 - 20 °C

5.1: dichloromethane / 2 h

6.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.17 h / 0 °C

6.2: 8 h / 20 °C

7.1: pyridine hydrogenfluoride / tetrahydrofuran / 2 h / 0 °C

With dmap; lithium hydroxide monohydrate; benzotriazol-1-ol; pyridine hydrogenfluoride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1016/j.tetlet.2014.04.079

Reference yield:

: 1610850-55-9
Boc-Ala-D-Phe(N-Me)-Gly(N-Me)-Ile-Ala(N-Me)-OMe

: 1610850-91-3
C₅₄H₈₁N₅O₁₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: lithium hydroxide monohydrate / tetrahydrofuran; methanol; water / 1 h / 0 - 20 °C

2.1: triethylamine; dmap / dichloromethane / 4 h / 0 - 20 °C

3.1: dichloromethane / 2 h

4.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.17 h / 0 °C

4.2: 8 h / 20 °C

5.1: pyridine hydrogenfluoride / tetrahydrofuran / 2 h / 0 °C

With dmap; lithium hydroxide monohydrate; benzotriazol-1-ol; pyridine hydrogenfluoride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1016/j.tetlet.2014.04.079