7-diethoxyphosphoryl-4,10-bis(2-nitrobenzenesulfonyl)-4,7,10,17-tetraazabicyclo[11.3.1]heptadeca-1⁽¹⁷⁾,13,15-triene

Base Information

• Chemical Name: 7-diethoxyphosphoryl-4,10-bis(2-nitrobenzenesulfonyl)-4,7,10,17-tetraazabicyclo[11.3.1]heptadeca-1⁽¹⁷⁾,13,15-triene
• CAS No.: 255383-21-2
• Molecular Formula: C₂₉H₃₇N₆O₁₁PS₂
• Molecular Weight: 740.752

Synonyms:7-diethoxyphosphoryl-4,10-bis(2-nitrobenzenesulfonyl)-4,7,10,17-tetraazabicyclo[11.3.1]heptadeca-1⁽¹⁷⁾,13,15-triene

Chemical Property of 7-diethoxyphosphoryl-4,10-bis(2-nitrobenzenesulfonyl)-4,7,10,17-tetraazabicyclo[11.3.1]heptadeca-1⁽¹⁷⁾,13,15-triene

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Technology Process of 7-diethoxyphosphoryl-4,10-bis(2-nitrobenzenesulfonyl)-4,7,10,17-tetraazabicyclo[11.3.1]heptadeca-1⁽¹⁷⁾,13,15-triene

There total 1 articles about 7-diethoxyphosphoryl-4,10-bis(2-nitrobenzenesulfonyl)-4,7,10,17-tetraazabicyclo[11.3.1]heptadeca-1⁽¹⁷⁾,13,15-triene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.0%

2,6-bis[N-(2-nitrobenzenesulfonyl)-2-aminoethyl]pyridine (255383-20-1) + N-(diethoxyphosphoryl)-O,O'-bis(2-methylsulfonyl)di-ethanolamine (166303-07-7) → 7-diethoxyphosphoryl-4,10-bis(2-nitrobenzenesulfonyl)-4,7,10,17-tetraazabicyclo[11.3.1]heptadeca-1(17),13,15-triene (255383-21-2)

Guidance literature:

With caesium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 40h; Inert atmosphere;

DOI:10.1021/jm901530b

Reference yield: 88.0%

7-diethoxyphosphoryl-4,10-bis(2-nitrobenzenesulfonyl)-4,7,10,17-tetraazabicyclo[11.3.1]heptadeca-1(17),13,15-triene (255383-21-2) → 4,10-bis(2-nitrobenzenesulfonyl)-4,7,10,17-tetraazabicyclo[11.3.1]heptadeca-1(17),13,15-triene (255383-22-3)

Guidance literature:

With hydrogen bromide; In acetic acid; at 20 ℃; for 22h;

DOI:10.1021/jm901530b

Reference yield: 52.0%

7-diethoxyphosphoryl-4,10-bis(2-nitrobenzenesulfonyl)-4,7,10,17-tetraazabicyclo[11.3.1]heptadeca-1(17),13,15-triene (255383-21-2) → 7-diethoxyphosphoryl-10-(2-nitrobenzenesulfonyl)-4,7,10,17-tetraazabicyclo[11.3.1]heptadeca-1(17),13,15-triene (255383-31-4)

Guidance literature:

With potassium carbonate; thiophenol; In N,N-dimethyl-formamide; at 20 - 50 ℃; for 2.5h; Inert atmosphere;

DOI:10.1021/jm901530b

upstream raw materials:

2,6-bis[N-(2-nitrobenzenesulfonyl)-2-aminoethyl]pyridine

N-(diethoxyphosphoryl)-O,O'-bis(2-methylsulfonyl)di-ethanolamine

Downstream raw materials:

7-diethoxyphosphoryl-10-(2-nitrobenzenesulfonyl)-4,7,10,17-tetraazabicyclo[11.3.1]heptadeca-1⁽¹⁷⁾,13,15-triene

4,10-bis(2-nitrobenzenesulfonyl)-4,7,10,17-tetraazabicyclo[11.3.1]heptadeca-1⁽¹⁷⁾,13,15-triene

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