C₁₃H₉BrClNO₃

Base Information

• Chemical Name: C₁₃H₉BrClNO₃
• CAS No.: 1002471-58-0
• Molecular Formula: C₁₃H₉BrClNO₃
• Molecular Weight: 342.576
• Mol file: 1002471-58-0.mol

Synonyms:C₁₃H₉BrClNO₃

Chemical Property of C₁₃H₉BrClNO₃

Chemical Property:

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Technology Process of C₁₃H₉BrClNO₃

There total 1 articles about C₁₃H₉BrClNO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-chloro-4-nitrophenol (619-08-9) + meta-bromobenzyl bromide (823-78-9) → C13H9BrClNO3 (1002471-58-0)

Guidance literature:

With potassium carbonate; In acetonitrile; at 25 - 50 ℃; for 12h;

DOI:10.1021/jm400349k

Reference yield: 48.0%

N,N-dimethylformamide diisopropyl acetal (18503-89-4) + C13H9BrClNO3 (1002471-58-0) → 3-[(2-chloro-4-nitrophenoxy)methyl]-N,N-dimethylbenzamide (50508-50-4)

Guidance literature:

With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In N,N-dimethyl-formamide; at 100 ℃; for 18h;

DOI:10.1002/hlca.202100162

Reference yield:

C13H9BrClNO3 (1002471-58-0) → 4-((3-bromobenzyl)oxy)-3-chloroaniline (1016801-85-6)

Guidance literature:

With ammonium chloride; zinc; In methanol; water; at 25 - 50 ℃; for 6h;

DOI:10.1021/jm400349k

upstream raw materials:

2-chloro-4-nitrophenol

meta-bromobenzyl bromide

Downstream raw materials:

4-((3-bromobenzyl)oxy)-3-chloroaniline

3-[(2-chloro-4-nitrophenoxy)methyl]-N,N-dimethylbenzamide