Technology Process of 5-(Benzyloxy)-2-iodo-4-methoxybenzaldehyde
There total 8 articles about 5-(Benzyloxy)-2-iodo-4-methoxybenzaldehyde which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
iodine; silver trifluoroacetate;
In
chloroform;
for 1h;
Ambient temperature;
- Guidance literature:
-
With
potassium carbonate;
In
N,N-dimethyl-formamide;
at 100 ℃;
for 2h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 41 percent / phenylmethanol; dimethylsulfoxide / 0.02 h / 150 °C
2: 42 percent / 2 percent NaOH / 1 h / 85 °C
3: 1.) FeSO4*7H2O, 25 percent NH4OH, 2.) 10 percent H2SO4, NaNO2, KI / 2.) CuI / 1.) 5 min, 100 deg C 2.) AcOH, H2O
With
ammonium hydroxide; sodium hydroxide; sulfuric acid; potassium iodide; sodium nitrite;
copper(l) iodide;
In
dimethyl sulfoxide; benzyl alcohol;