C₂₅H₂₆N₂O₆

Base Information

• Chemical Name: C₂₅H₂₆N₂O₆
• CAS No.: 943326-48-5
• Molecular Formula: C₂₅H₂₆N₂O₆
• Molecular Weight: 450.491
• Mol file: 943326-48-5.mol

Synonyms:C₂₅H₂₆N₂O₆

Chemical Property of C₂₅H₂₆N₂O₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₅H₂₆N₂O₆

There total 7 articles about C₂₅H₂₆N₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

C43H68N2O6Si3 (943326-47-4) → C25H26N2O6 (943326-48-5)

Guidance literature:

With amberlyst-15; In methanol; dichloromethane; at 20 ℃; for 2h;

DOI:10.1016/j.bmc.2007.03.054

Reference yield:

C27H53NO5Si3 (943326-45-2) → C25H26N2O6 (943326-48-5)

Guidance literature:

Multi-step reaction with 4 steps

1: 85 percent / ammonium formate / Pd/C / tetrahydrofuran; methanol / 2.5 h / 20 °C

2: toluene / 0.5 h / Heating

3: 751 mg / triethylamine / dimethylformamide / 1 h

4: 65 percent / Amberlyst-15 / methanol; CH₂Cl₂ / 2 h / 20 °C

With amberlyst-15; ammonium formate; triethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; toluene;

DOI:10.1016/j.bmc.2007.03.054

Reference yield:

1,3,5-tris(hydroxymethyl)benzene (4464-18-0) → C25H26N2O6 (943326-48-5)

Guidance literature:

Multi-step reaction with 6 steps

1: 68 percent / imidazole / dimethylformamide / 0 - 20 °C

2: 75 percent / acetic anhydride; nitric acid / -20 - 0 °C

3: 85 percent / ammonium formate / Pd/C / tetrahydrofuran; methanol / 2.5 h / 20 °C

4: toluene / 0.5 h / Heating

5: 751 mg / triethylamine / dimethylformamide / 1 h

6: 65 percent / Amberlyst-15 / methanol; CH₂Cl₂ / 2 h / 20 °C

With 1H-imidazole; amberlyst-15; nitric acid; ammonium formate; acetic anhydride; triethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; toluene;

DOI:10.1016/j.bmc.2007.03.054

upstream raw materials:

C₄₃H₆₈N₂O₆Si₃

C₂₇H₅₃NO₅Si₃

C₂₇H₅₅NO₃Si₃

1,3,5-tris(hydroxymethyl)benzene

Downstream raw materials:

C₄₆H₃₅N₅O₁₈