2-{2-[2-(2-nitro-4-methoxycarbonylbenzoylamino)benzoylamino]-4-methoxycarbonylbenzoylamino}benzoic acid 1-hexyl ester

Base Information

Chemical Name:2-{2-[2-(2-nitro-4-methoxycarbonylbenzoylamino)benzoylamino]-4-methoxycarbonylbenzoylamino}benzoic acid 1-hexyl ester
CAS No.:180133-10-2
Molecular Formula:C₃₈H₃₆N₄O₁₁
Molecular Weight:724.724
Hs Code.:

Synonyms:2-{2-[2-(2-nitro-4-methoxycarbonylbenzoylamino)benzoylamino]-4-methoxycarbonylbenzoylamino}benzoic acid 1-hexyl ester

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Chemical Property of 2-{2-[2-(2-nitro-4-methoxycarbonylbenzoylamino)benzoylamino]-4-methoxycarbonylbenzoylamino}benzoic acid 1-hexyl ester

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Technology Process of 2-{2-[2-(2-nitro-4-methoxycarbonylbenzoylamino)benzoylamino]-4-methoxycarbonylbenzoylamino}benzoic acid 1-hexyl ester

There total 12 articles about 2-{2-[2-(2-nitro-4-methoxycarbonylbenzoylamino)benzoylamino]-4-methoxycarbonylbenzoylamino}benzoic acid 1-hexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 51919-74-5
4-chlorocarbonyl-3-nitrobenzoic acid methyl ester

: 180133-09-9
2-[2-(2-aminobenzoylamino)-4-methoxycarbonylbenzoylamino]benzoic acid 1-hexyl ester

: 180133-10-2
2-{2-[2-(2-nitro-4-methoxycarbonylbenzoylamino)benzoylamino]-4-methoxycarbonylbenzoylamino}benzoic acid 1-hexyl ester

Guidance literature:: With pyridine; In dichloromethane; Ambient temperature;
DOI:10.1021/ja9539857

Reference yield:

: 552-16-9,104810-18-6
ortho-nitrobenzoic acid

: 180133-10-2
2-{2-[2-(2-nitro-4-methoxycarbonylbenzoylamino)benzoylamino]-4-methoxycarbonylbenzoylamino}benzoic acid 1-hexyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: oxalyl chloride, DMF / CH₂Cl₂ / 4 h / Ambient temperature

2: 78 percent / pyridine / CH₂Cl₂ / Ambient temperature

3: 100 percent / H₂ / 10percent Pd/C / CH₂Cl₂ / Ambient temperature

4: 62 percent / pyridine / CH₂Cl₂ / Ambient temperature

With pyridine; oxalyl dichloride; hydrogen; N,N-dimethyl-formamide; palladium on activated charcoal; In dichloromethane;
DOI:10.1021/ja9539857

Reference yield:

: 610-29-7
2-nitroterephthalic acid

: 180133-10-2
2-{2-[2-(2-nitro-4-methoxycarbonylbenzoylamino)benzoylamino]-4-methoxycarbonylbenzoylamino}benzoic acid 1-hexyl ester

Guidance literature:: Multi-step reaction with 7 steps

1: 71 percent / H₂SO₄ / 1.25 h / Heating

2: oxalyl chloride, DMF / tetrahydrofuran / 0.5 h / Ambient temperature

3: 89 percent / pyridine / CH₂Cl₂ / Ambient temperature

4: H₂ / 10percent Pd/C / CH₂Cl₂ / Ambient temperature

5: 78 percent / pyridine / CH₂Cl₂ / Ambient temperature

6: 100 percent / H₂ / 10percent Pd/C / CH₂Cl₂ / Ambient temperature

7: 62 percent / pyridine / CH₂Cl₂ / Ambient temperature

With pyridine; oxalyl dichloride; sulfuric acid; hydrogen; N,N-dimethyl-formamide; palladium on activated charcoal; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja9539857