4-HYDROXYIMINOMETHYL-1,2,5,5-PENTAMETHYL-3-IMIDAZOLINE-3-OXIDE

Base Information

• Chemical Name: 4-HYDROXYIMINOMETHYL-1,2,5,5-PENTAMETHYL-3-IMIDAZOLINE-3-OXIDE
• CAS No.: 70183-45-8
• Molecular Formula: C₉H₁₇N₃O₂
• Molecular Weight: 199.253
• Hs Code.: 2933299090
• Mol file: 70183-45-8.mol

Synonyms:4-HYDROXYIMINOMETHYL-1,2,5,5-PENTAMETHYL-3-IMIDAZOLINE-3-OXIDE;4-[(Hydroxyimino)methyl]-1,2,2,5,5-pentamethyl-3-imidazoline-3-oxide

Chemical Property of 4-HYDROXYIMINOMETHYL-1,2,5,5-PENTAMETHYL-3-IMIDAZOLINE-3-OXIDE

Chemical Property:

• Melting Point: 183-186ºC
• PSA: 64.58000
• LogP: 0.75450

Purity/Quality:

99% ^*data from raw suppliers

4-[(HYDROXYIMINO)METHYL]-1,2,2,5,5-PENTAMETHYL-3-IMIDAZOLINE-3-OXIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-HYDROXYIMINOMETHYL-1,2,5,5-PENTAMETHYL-3-IMIDAZOLINE-3-OXIDE

There total 7 articles about 4-HYDROXYIMINOMETHYL-1,2,5,5-PENTAMETHYL-3-IMIDAZOLINE-3-OXIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

1,2,2,5,5-pentamethyl-4-dimethoxymethyl-3-imidazoline-3-oxide (90277-71-7) → 1,2,2,5,5-pentamethyl-4-hydroxyiminomethyl-3-imidazoline-3-oxide (70183-45-8)

Guidance literature:

With hydroxylamine hydrochloride; In ethanol; for 240h;

DOI:10.1007/BF01157344

Reference yield: 70.0%

C9H17LiN2O → 1,2,2,5,5-pentamethyl-4-hydroxyiminomethyl-3-imidazoline-3-oxide (70183-45-8)

Guidance literature:

With n-Amyl nitrite; at 20 ℃; for 1h;

DOI:10.1007/BF00958816

Reference yield: 70.0%

1,2,2,5,5-pentamethyl-4-diethoxymethyl-3-imidazoline-3-oxide → 1,2,2,5,5-pentamethyl-4-hydroxyiminomethyl-3-imidazoline-3-oxide (70183-45-8)

Guidance literature:

With hydroxylamine hydrochloride; In ethanol; for 240h;

DOI:10.1007/BF01157344

upstream raw materials:

1,2,2,5,5-pentamethyl-4-dimethoxymethyl-3-imidazoline-3-oxide

1,2,2,5,5-pentamethyl-4-formyl-3-imidazolin-3-oxide

4-dibromomethyl-1,2,2,5,5-pentamethyl-3-imidazoline-3-oxide

Downstream raw materials:

2,2,5,5-tetramethyl-4-hydroxyiminomethyl-3-imidazoline-3-oxide-1-oxyl