1-HYDROXY-4-[(HYDROXYIMINO)METHYL]-2,2,5,5-TETRAMETHYL-2,5-DIHYDRO-1H-IMIDAZOL-3-IUM-3-OLATE

Base Information

• Chemical Name: 1-HYDROXY-4-[(HYDROXYIMINO)METHYL]-2,2,5,5-TETRAMETHYL-2,5-DIHYDRO-1H-IMIDAZOL-3-IUM-3-OLATE
• CAS No.: 49837-80-1
• Molecular Formula: C₈H₁₅N₃O₃
• Molecular Weight: 201.225
• Mol file: 49837-80-1.mol

Synonyms:4-[(Hydroxyimino)methyl]-2,2,5,5-tetramethyl-2,5-dihydro-1H-imidazol-1-ol 3-oxide;

Chemical Property of 1-HYDROXY-4-[(HYDROXYIMINO)METHYL]-2,2,5,5-TETRAMETHYL-2,5-DIHYDRO-1H-IMIDAZOL-3-IUM-3-OLATE

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Melting Point: 162-164 °C
• Refractive Index: 1.554
• Boiling Point: 381.5 °C at 760 mmHg
• Flash Point: 184.5 °C
• PSA: 84.81000
• Density: 1.27 g/cm³
• LogP: 0.51390

Purity/Quality:

98%min ^*data from raw suppliers

1-HYDROXY-2,2,5,5-TETRAMETHYL-4-[(HYDROXYIMINO)METHYL]IMIDAZOLE-3-OXIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-HYDROXY-4-[(HYDROXYIMINO)METHYL]-2,2,5,5-TETRAMETHYL-2,5-DIHYDRO-1H-IMIDAZOL-3-IUM-3-OLATE

There total 3 articles about 1-HYDROXY-4-[(HYDROXYIMINO)METHYL]-2,2,5,5-TETRAMETHYL-2,5-DIHYDRO-1H-IMIDAZOL-3-IUM-3-OLATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 23.0%

methylhydrazine hemisulfate (302-15-8,5118-34-3) + 4-Hydroxyiminomethylen-2,2,5,5-tetramethyl-3-imidazolin-1-oxyl-3-oxid (49837-81-2) → 1-methoxy-4-hydroxyiminomethyl-2,2,5,5-tetramethyl-3-imidazoline-3-oxide (88571-36-2) + 1-Hydroxy-4-hydroxyiminomethylen-2,2,5,5-tetramethyl-3-imidazolin-3-oxid (49837-80-1)

Guidance literature:

With triethylamine; In methanol; for 0.5h;

DOI:10.1007/BF00955785

Reference yield:

→ 1-Hydroxy-4-hydroxyiminomethylen-2,2,5,5-tetramethyl-3-imidazolin-3-oxid (49837-80-1)

Guidance literature:

1-Hydroxy-2,2,4,5,5-pentamethyl-3-imidazolin-3-oxid, NaNH2, Amylnitrit;

Reference yield:

→ 1-hydroxy-2,2,5,5-tetramethyl-3-oxy-2,5-dihydro-1H-imidazole-4-carbaldehyde oxime (49837-80-1)

Guidance literature:

Imidazolin I, NH2OH;

upstream raw materials:

methylhydrazine hemisulfate

4-Hydroxyiminomethylen-2,2,5,5-tetramethyl-3-imidazolin-1-oxyl-3-oxid

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