(S)-1-allyl 4-((S)-3-(allyloxy)-2-(((benzyloxy)carbonyl)amino)-3-oxopropyl) 2-(((benzyloxy)carbonyl)amino)succinate

Base Information

Chemical Name:(S)-1-allyl 4-((S)-3-(allyloxy)-2-(((benzyloxy)carbonyl)amino)-3-oxopropyl) 2-(((benzyloxy)carbonyl)amino)succinate
CAS No.:1415903-51-3
Molecular Formula:C₂₉H₃₂N₂O₁₀
Molecular Weight:568.58
Hs Code.:

Synonyms:(S)-1-allyl 4-((S)-3-(allyloxy)-2-(((benzyloxy)carbonyl)amino)-3-oxopropyl) 2-(((benzyloxy)carbonyl)amino)succinate

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Chemical Property of (S)-1-allyl 4-((S)-3-(allyloxy)-2-(((benzyloxy)carbonyl)amino)-3-oxopropyl) 2-(((benzyloxy)carbonyl)amino)succinate

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Technology Process of (S)-1-allyl 4-((S)-3-(allyloxy)-2-(((benzyloxy)carbonyl)amino)-3-oxopropyl) 2-(((benzyloxy)carbonyl)amino)succinate

There total 1 articles about (S)-1-allyl 4-((S)-3-(allyloxy)-2-(((benzyloxy)carbonyl)amino)-3-oxopropyl) 2-(((benzyloxy)carbonyl)amino)succinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 88295-41-4
N-(benzyloxycarbonyl)serine allyl ester

: 127949-87-5
(S)-4-(allyloxy)-3-(((benzyloxy)carbonyl)amino)-4-oxobutanoic acid

: 1415903-51-3
(S)-1-allyl 4-((S)-3-(allyloxy)-2-(((benzyloxy)carbonyl)amino)-3-oxopropyl) 2-(((benzyloxy)carbonyl)amino)succinate

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 0 ℃;
DOI:10.3109/14756366.2011.604319

Reference yield:

: 1415903-51-3
(S)-1-allyl 4-((S)-3-(allyloxy)-2-(((benzyloxy)carbonyl)amino)-3-oxopropyl) 2-(((benzyloxy)carbonyl)amino)succinate

: 1415903-52-4
(S)-2-(((benzyloxy)carbonyl)amino)-4-((S)-2-(((benzyloxy)carbonyl)amino)-2-carboxyethoxy)-4-oxobutanoic acid

Guidance literature:: With morpholine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; at 20 ℃; for 1.5h; Inert atmosphere;
DOI:10.3109/14756366.2011.604319

Reference yield:

: 1415903-51-3
(S)-1-allyl 4-((S)-3-(allyloxy)-2-(((benzyloxy)carbonyl)amino)-3-oxopropyl) 2-(((benzyloxy)carbonyl)amino)succinate

: (9S,14S)-9,14-bis(((benzyloxy)carbonyl)amino)-5,8,12,15,18-pentaoxo-N¹,N²²-dipropyl-7,11,16-trioxa-4,19-diazadocosane-1,22-diaminium 2,2,2-trifluoroacetate

Guidance literature:: Multi-step reaction with 3 steps

1: morpholine; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran / 1.5 h / 20 °C / Inert atmosphere

2: N-ethyl-N,N-diisopropylamine; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one / tetrahydrofuran

3: dichloromethane / 2 h / Inert atmosphere

With morpholine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; N-ethyl-N,N-diisopropylamine; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; In tetrahydrofuran; dichloromethane;
DOI:10.3109/14756366.2011.604319