N-(benzyloxycarbonyl)iminodiacetaldehyde

Base Information

• Chemical Name: N-(benzyloxycarbonyl)iminodiacetaldehyde
• CAS No.: 127747-10-8
• Molecular Formula: C₁₂H₁₃NO₄
• Molecular Weight: 235.24

Synonyms:N-(benzyloxycarbonyl)iminodiacetaldehyde

Chemical Property of N-(benzyloxycarbonyl)iminodiacetaldehyde

Chemical Property:

Purity/Quality:

99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of N-(benzyloxycarbonyl)iminodiacetaldehyde

There total 4 articles about N-(benzyloxycarbonyl)iminodiacetaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

3,4-cis-dihydroxy-pyrrolidine-1-carboxylic acid benzyl ester → N-(benzyloxycarbonyl)iminodiacetaldehyde (127747-10-8)

Guidance literature:

With sodium periodate; In tetrahydrofuran; water; at 20 ℃; for 0.5h;

Reference yield: 82.0%

3,4-cis-dihydroxy-pyrrolidine-1-carboxylic acid benzyl ester (122225-42-7) → N-(benzyloxycarbonyl)iminodiacetaldehyde (127747-10-8)

Guidance literature:

With sodium periodate; In tetrahydrofuran; water; at 20 ℃; for 0.0833333h;

DOI:10.1055/S-0029-1218622

Reference yield: 75.0%

1-carboxybenzyl-3-pyrrolidine (31970-04-4) → N-(benzyloxycarbonyl)iminodiacetaldehyde (127747-10-8)

Guidance literature:

With 2,6-dimethylpyridine; potassium osmate(VI) dihydrate; sodium periodate; In ethyl acetate; at 0 - 20 ℃; for 3h;

upstream raw materials:

3,4-cis-dihydroxy-pyrrolidine-1-carboxylic acid benzyl ester

1-carboxybenzyl-3-pyrrolidine

(3S,4S)-N-benzyloxycarbonyl-3,4-dihydroxy-pyrrolidine

Downstream raw materials:

benzyl 4-(2,2,2-trifluoroethyl)piperazine-1-carboxylate

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