C₄₂H₈₂O₇Si₃

Base Information

Chemical Name:C₄₂H₈₂O₇Si₃
CAS No.:942505-92-2
Molecular Formula:C₄₂H₈₂O₇Si₃
Molecular Weight:783.365
Hs Code.:

C<sub>42</sub>H<sub>82</sub>O<sub>7</sub>Si<sub>3</sub>

Synonyms:C₄₂H₈₂O₇Si₃

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Chemical Property of C₄₂H₈₂O₇Si₃

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Technology Process of C₄₂H₈₂O₇Si₃

There total 18 articles about C₄₂H₈₂O₇Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 942505-91-1
C₄₂H₈₀O₇Si₃

: 942505-92-2
C₄₂H₈₂O₇Si₃

: 942505-93-3
C₃₄H₇₄O₆Si₃

Guidance literature:: With dimethylsulfide borane complex; In toluene; at 100 ℃;
DOI:10.1039/b700827a

Reference yield:

: 942505-86-4
C₁₄H₃₀O₂Si

: 942505-92-2
C₄₂H₈₂O₇Si₃

Guidance literature:: Multi-step reaction with 9 steps

1.1: 91 percent / Grubbs catalyst (second generation) / CH₂Cl₂

2.1: KO-t-Bu / tetrahydrofuran / -20 °C

3.1: LiAlH₄ / diethyl ether

4.1: Dess-Martin periodinane / CH₂Cl₂

5.1: 80 percent / TiCl₄ / CH₂Cl₂ / -78 °C

6.1: imidazole; DMAP / dimethylformamide

6.2: O₃ / CH₂Cl₂ / -78 °C

6.3: 85 percent / PPh₃ / CH₂Cl₂

7.1: (-)-Ipc₂BCl; Et₃N / diethyl ether

7.2: 75 percent / diethyl ether / -78 °C

8.1: Me₄NBH(OAc)3; AcOH / acetonitrile / -30 °C

8.2: DDQ; 4 Angstroem molecular sieves / CH₂Cl₂

8.3: 51 percent / 2,6-lutidine / CH₂Cl₂

9.1: 62 percent / BH₃*Me₂S / toluene / 100 °C

With 1H-imidazole; dmap; lithium aluminium tetrahydride; dimethylsulfide borane complex; potassium tert-butylate; titanium tetrachloride; Dess-Martin periodane; acetic acid; triethylamine; (-)-diisopinocamphenylborane chloride; tetramethylammonium triacetoxyborohydride; Grubbs catalyst (second generation); In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile; 2.1: intramolecular Michael addition;
DOI:10.1039/b700827a

Reference yield:

: 95337-97-6,95338-04-8,110171-85-2,130659-83-5
2-[2-[[(tert-butyl)dimethylsilyl]oxy]ethyl]oxirane

: 942505-92-2
C₄₂H₈₂O₇Si₃

Guidance literature:: Multi-step reaction with 11 steps

1.1: (S,S)-(salen)Co(II); AcOH; H₂O / kinetic racemate resolution

2.1: 96 percent / CuI / tetrahydrofuran

3.1: 91 percent / Grubbs catalyst (second generation) / CH₂Cl₂

4.1: KO-t-Bu / tetrahydrofuran / -20 °C

5.1: LiAlH₄ / diethyl ether

6.1: Dess-Martin periodinane / CH₂Cl₂

7.1: 80 percent / TiCl₄ / CH₂Cl₂ / -78 °C

8.1: imidazole; DMAP / dimethylformamide

8.2: O₃ / CH₂Cl₂ / -78 °C

8.3: 85 percent / PPh₃ / CH₂Cl₂

9.1: (-)-Ipc₂BCl; Et₃N / diethyl ether

9.2: 75 percent / diethyl ether / -78 °C

10.1: Me₄NBH(OAc)3; AcOH / acetonitrile / -30 °C

10.2: DDQ; 4 Angstroem molecular sieves / CH₂Cl₂

10.3: 51 percent / 2,6-lutidine / CH₂Cl₂

11.1: 62 percent / BH₃*Me₂S / toluene / 100 °C

With 1H-imidazole; dmap; copper(l) iodide; lithium aluminium tetrahydride; dimethylsulfide borane complex; potassium tert-butylate; water; titanium tetrachloride; Dess-Martin periodane; acetic acid; triethylamine; (-)-diisopinocamphenylborane chloride; tetramethylammonium triacetoxyborohydride; Grubbs catalyst (second generation); In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile; 1.1: Jacobsen hydrolytic kinetic resolution / 4.1: intramolecular Michael addition;
DOI:10.1039/b700827a