1-(1-Benzothiophen-2-yl)-2-bromo-1-ethanone

Base Information

Chemical Name:1-(1-Benzothiophen-2-yl)-2-bromo-1-ethanone
CAS No.:97511-06-3
Molecular Formula:C10H7BrOS
Molecular Weight:255.135
Hs Code.:2934999090
European Community (EC) Number:843-745-4
DSSTox Substance ID:DTXSID00383603
Nikkaji Number:J865.732G
Wikidata:Q82175389
Mol file:97511-06-3.mol

Synonyms:97511-06-3;1-(1-Benzothiophen-2-yl)-2-bromo-1-ethanone;1-(1-benzothiophen-2-yl)-2-bromoethanone;1-(1-Benzothiophen-2-yl)-2-bromoethan-1-one;1-(BENZOTHIOPHEN-2-YL)-2-BROMOETHAN-1-ONE;1-(benzo[b]thiophen-2-yl)-2-bromoethanone;2-(Bromoacetyl)benzo[b]thiophene;1-(Benzo[b]thiophen-2-yl)-2-bromoethan-1-one;SCHEMBL231135;DTXSID00383603;WVTSOGFICBVCRE-UHFFFAOYSA-N;MFCD06658971;AKOS017560276;MS-22190;CS-0236315;1-(1-BENZOTHIEN-2-YL)-2-BROMOETHANONE;EN300-1702994;J-502843

Suppliers and Price of 1-(1-Benzothiophen-2-yl)-2-bromo-1-ethanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

SynQuest Laboratories
2-(Bromoacetyl)benzo[b]thiophene
5 g
$ 1000.00

SynQuest Laboratories
2-(Bromoacetyl)benzo[b]thiophene
1 g
$ 256.00

SynQuest Laboratories
2-(Bromoacetyl)benzo[b]thiophene
250 mg
$ 144.00

Apolloscientific
2-(Bromoacetyl)benzo[b]thiophene
250mg
$ 131.00

Apolloscientific
2-(Bromoacetyl)benzo[b]thiophene
1g
$ 232.00

Apolloscientific
2-(Bromoacetyl)benzo[b]thiophene
5g
$ 907.00

American Custom Chemicals Corporation
1-(1-BENZOTHIOPHEN-2-YL)-2-BROMO-1-ETHANONE 95.00%
1G
$ 766.69

American Custom Chemicals Corporation
1-(1-BENZOTHIOPHEN-2-YL)-2-BROMO-1-ETHANONE 95.00%
250MG
$ 661.91

AK Scientific
1-(1-Benzothiophen-2-yl)-2-bromo-1-ethanone
10g
$ 1415.00

AK Scientific
1-(1-Benzothiophen-2-yl)-2-bromo-1-ethanone
1g
$ 428.00

Total 9 raw suppliers

Chemical Property of 1-(1-Benzothiophen-2-yl)-2-bromo-1-ethanone

Chemical Property:

Vapor Pressure:3.96E-05mmHg at 25°C
Melting Point:117.5-118.5 °C
Refractive Index:1.689
Boiling Point:352 °C at 760 mmHg
Flash Point:166.7 °C
PSA：45.31000
Density:1.617 g/cm³
LogP:3.47890
XLogP3:3.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:253.94010
Heavy Atom Count:13
Complexity:207

Purity/Quality:

98%min ^*data from raw suppliers

2-(Bromoacetyl)benzo[b]thiophene ^*data from reagent suppliers

Safty Information:

Pictogram(s): C
Hazard Codes:C

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C2C(=C1)C=C(S2)C(=O)CBr

Technology Process of 1-(1-Benzothiophen-2-yl)-2-bromo-1-ethanone

There total 3 articles about 1-(1-Benzothiophen-2-yl)-2-bromo-1-ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 22720-75-8
2-acetyl benzo[b]thiophene

: 97511-06-3
1-(benzo[b]thiophen-2-yl)-2-bromoethanone

Guidance literature:: With tetra-N-butylammonium tribromide; In methanol; dichloromethane; at 20 ℃; for 15h; Product distribution / selectivity;

Reference yield:

: 95-15-8,11095-43-5
Benzo[b]thiophene

: 97511-06-3
1-(benzo[b]thiophen-2-yl)-2-bromoethanone

Guidance literature:: Multi-step reaction with 2 steps

1: 35 percent / n-BuLi / tetrahydrofuran; hexane / -78 - 22 °C

2: 95 percent / (n-Bu)4NBr₃ / CH₂Cl₂; methanol / 6 h / 22 °C

With n-butyllithium; tetrabuthylammonium tribromide; In tetrahydrofuran; methanol; hexane; dichloromethane;
DOI:10.3987/com-97-7820