(2S,3S)-N-benzoyl-2-methoxycarbonyl-3-methoxycarbonylmethyl-4-phenyl-<4,5>-dehydropyrrolidine

Base Information

Chemical Name:(2S,3S)-N-benzoyl-2-methoxycarbonyl-3-methoxycarbonylmethyl-4-phenyl-<4,5>-dehydropyrrolidine
CAS No.:169774-75-8
Molecular Formula:C₂₂H₂₁NO₅
Molecular Weight:379.412
Hs Code.:

Synonyms:(2S,3S)-N-benzoyl-2-methoxycarbonyl-3-methoxycarbonylmethyl-4-phenyl-<4,5>-dehydropyrrolidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3S)-N-benzoyl-2-methoxycarbonyl-3-methoxycarbonylmethyl-4-phenyl-<4,5>-dehydropyrrolidine

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Technology Process of (2S,3S)-N-benzoyl-2-methoxycarbonyl-3-methoxycarbonylmethyl-4-phenyl-<4,5>-dehydropyrrolidine

There total 3 articles about (2S,3S)-N-benzoyl-2-methoxycarbonyl-3-methoxycarbonylmethyl-4-phenyl-<4,5>-dehydropyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: 189573-89-5
(2S,3S)-1-Benzoyl-3-carboxymethyl-4-phenyl-2,3-dihydro-1H-pyrrole-2-carboxylic acid methyl ester

: 169774-75-8
(2S,3S)-N-benzoyl-2-methoxycarbonyl-3-methoxycarbonylmethyl-4-phenyl-<4,5>-dehydropyrrolidine

Guidance literature:: In diethyl ether; dichloromethane; for 2h; Ambient temperature;
DOI:10.1016/S0040-4020(97)00191-9

Reference yield:

: 169774-65-6
(2S,3S)-N-benzoyl-2-methoxycarbonyl-3-tert-butoxycarbonylmethyl-4-phenyl-<4,5>-dehydropyrrolidine

: 169774-75-8
(2S,3S)-N-benzoyl-2-methoxycarbonyl-3-methoxycarbonylmethyl-4-phenyl-<4,5>-dehydropyrrolidine

Guidance literature:: Multi-step reaction with 2 steps

1: CF₃CO₂H, anisole / toluene / Ambient temperature

2: 90 percent / CH₂Cl₂; diethyl ether / 2 h / Ambient temperature

With methoxybenzene; trifluoroacetic acid; In diethyl ether; dichloromethane; toluene;
DOI:10.1016/S0040-4020(97)00191-9