Technology Process of C26H15Br2ClO
There total 4 articles about C26H15Br2ClO which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
thionyl chloride;
In
toluene;
for 24h;
Inert atmosphere;
Reflux;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: acetic anhydride / Reflux
1.2: 1 h / 60 °C / Reflux
2.1: tetrahydrofuran; dibutyl ether / 2 h / -78 - 20 °C / Inert atmosphere
3.1: trifluoroacetic acid / chlorobenzene / 48 h / Reflux
4.1: thionyl chloride / toluene / 24 h / Inert atmosphere; Reflux
With
thionyl chloride; acetic anhydride; trifluoroacetic acid;
In
tetrahydrofuran; dibutyl ether; chlorobenzene; toluene;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: tetrahydrofuran; dibutyl ether / 2 h / -78 - 20 °C / Inert atmosphere
2: trifluoroacetic acid / chlorobenzene / 48 h / Reflux
3: thionyl chloride / toluene / 24 h / Inert atmosphere; Reflux
With
thionyl chloride; trifluoroacetic acid;
In
tetrahydrofuran; dibutyl ether; chlorobenzene; toluene;