N-<2-(5,5-diphenyl-2,4-imidazolidinedion-3-yl)ethyl>-7-acetoxy-1-naphthalene sulfonamide

Base Information

Chemical Name:N-<2-(5,5-diphenyl-2,4-imidazolidinedion-3-yl)ethyl>-7-acetoxy-1-naphthalene sulfonamide
CAS No.:92220-76-3
Molecular Formula:C₂₉H₂₅N₃O₆S
Molecular Weight:543.6
Hs Code.:

Synonyms:N-<2-(5,5-diphenyl-2,4-imidazolidinedion-3-yl)ethyl>-7-acetoxy-1-naphthalene sulfonamide

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Chemical Property of N-<2-(5,5-diphenyl-2,4-imidazolidinedion-3-yl)ethyl>-7-acetoxy-1-naphthalene sulfonamide

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Technology Process of N-<2-(5,5-diphenyl-2,4-imidazolidinedion-3-yl)ethyl>-7-acetoxy-1-naphthalene sulfonamide

There total 5 articles about N-<2-(5,5-diphenyl-2,4-imidazolidinedion-3-yl)ethyl>-7-acetoxy-1-naphthalene sulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 92241-05-9
2-acetoxy-8-naphthalenesulfonyl chloride

: 14046-88-9
3-(2-aminoethyl)-5,5-diphenylhydantoin

: 92220-76-3
N-<2-(5,5-diphenyl-2,4-imidazolidinedion-3-yl)ethyl>-7-acetoxy-1-naphthalene sulfonamide

Guidance literature:: With triethylamine; In acetone; for 0.5h; Ambient temperature;
DOI:10.1021/ac00278a061

Reference yield:

: 57-41-0
phenythoin

: 92220-76-3
N-<2-(5,5-diphenyl-2,4-imidazolidinedion-3-yl)ethyl>-7-acetoxy-1-naphthalene sulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / dimethylformamide / 2 h / Heating

2: 65 percent / methylamine / H₂O; methanol / 48 h

3: 60 percent / triethylamine / acetone / 0.5 h / Ambient temperature

With triethylamine; methylamine; In methanol; water; N,N-dimethyl-formamide; acetone;
DOI:10.1021/ac00278a061

Reference yield:

: 832-85-9
2-hydroxy-8-naphthalenesulfonic acid monosodium salt

: 92220-76-3
N-<2-(5,5-diphenyl-2,4-imidazolidinedion-3-yl)ethyl>-7-acetoxy-1-naphthalene sulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: 78 percent / sodium acetate / dimethylformamide / 3 h / 80 °C

2: 85 percent / thionyl chloride / Heating

3: 60 percent / triethylamine / acetone / 0.5 h / Ambient temperature

With thionyl chloride; sodium acetate; triethylamine; In N,N-dimethyl-formamide; acetone;
DOI:10.1021/ac00278a061