N'-[[2-[allyl(methyl)amino]-5-methoxy-1-(4-methylphenyl)-1H-pyrrol-3-yl]methylene]-4-methylbenzenesulfohydrazide

Base Information

Chemical Name:N'-[[2-[allyl(methyl)amino]-5-methoxy-1-(4-methylphenyl)-1H-pyrrol-3-yl]methylene]-4-methylbenzenesulfohydrazide
CAS No.:823197-95-1
Molecular Formula:C₂₄H₂₈N₄O₃S
Molecular Weight:452.577
Hs Code.:

Synonyms:N'-[[2-[allyl(methyl)amino]-5-methoxy-1-(4-methylphenyl)-1H-pyrrol-3-yl]methylene]-4-methylbenzenesulfohydrazide

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Chemical Property of N'-[[2-[allyl(methyl)amino]-5-methoxy-1-(4-methylphenyl)-1H-pyrrol-3-yl]methylene]-4-methylbenzenesulfohydrazide

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Technology Process of N'-[[2-[allyl(methyl)amino]-5-methoxy-1-(4-methylphenyl)-1H-pyrrol-3-yl]methylene]-4-methylbenzenesulfohydrazide

There total 2 articles about N'-[[2-[allyl(methyl)amino]-5-methoxy-1-(4-methylphenyl)-1H-pyrrol-3-yl]methylene]-4-methylbenzenesulfohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 280576-51-4
2-[allyl(methyl)amino]-5-methoxy-1-(4-methylphenyl)-1H-3-pyrrolecarbaldehyde

: 823197-95-1
N'-[[2-[allyl(methyl)amino]-5-methoxy-1-(4-methylphenyl)-1H-pyrrol-3-yl]methylene]-4-methylbenzenesulfohydrazide

Guidance literature:: With hydrogenchloride; In methanol; at 0 ℃; for 3h;

Reference yield:

: 280576-49-0
2-chloro-5-methoxy-1-(4-methylphenyl)-1H-3-pyrrolcarbaldehyde

: 823197-95-1
N'-[[2-[allyl(methyl)amino]-5-methoxy-1-(4-methylphenyl)-1H-pyrrol-3-yl]methylene]-4-methylbenzenesulfohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / ethanol / 10 h / Heating

2: 65 percent / aq. HCl / methanol / 3 h / 0 °C

With hydrogenchloride; In methanol; ethanol;