5,6-bis(4hydroxyphenyl)-2,3-dihydroimidazo<2,1-b>thiazole hydrobromide

Base Information

Chemical Name:5,6-bis(4hydroxyphenyl)-2,3-dihydroimidazo<2,1-b>thiazole hydrobromide
CAS No.:66659-78-7
Molecular Formula:BrH*C₁₇H₁₄N₂O₂S
Molecular Weight:391.288
Hs Code.:

Synonyms:5,6-bis(4hydroxyphenyl)-2,3-dihydroimidazo<2,1-b>thiazole hydrobromide

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Chemical Property of 5,6-bis(4hydroxyphenyl)-2,3-dihydroimidazo<2,1-b>thiazole hydrobromide

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Technology Process of 5,6-bis(4hydroxyphenyl)-2,3-dihydroimidazo<2,1-b>thiazole hydrobromide

There total 4 articles about 5,6-bis(4hydroxyphenyl)-2,3-dihydroimidazo<2,1-b>thiazole hydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 64997-22-4
2,3-dihydro-5,6-bis(p-methoxyphenyl)imidazo[2,1-b]thiazole

: 66659-78-7
5,6-bis(4hydroxyphenyl)-2,3-dihydroimidazo<2,1-b>thiazole hydrobromide

Guidance literature:: With boron tribromide; In dichloromethane; Ambient temperature;
DOI:10.1021/jm00147a008

Reference yield:

: 27895-95-0
2-bromo-1,2-bis(4-methoxyphenyl)ethanone

: 66659-78-7
5,6-bis(4hydroxyphenyl)-2,3-dihydroimidazo<2,1-b>thiazole hydrobromide

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / K₂CO₃ / acetonitrile / 18 h / Ambient temperature

2: 52 percent / BBr₃ / CH₂Cl₂ / Ambient temperature

With boron tribromide; potassium carbonate; In dichloromethane; acetonitrile;
DOI:10.1021/jm00147a008

Reference yield:

: 39908-69-5
4,5-bis(4-methoxyphenyl)-1,3-dihydro-imidazole-2-thione

: 66659-78-7
5,6-bis(4hydroxyphenyl)-2,3-dihydroimidazo<2,1-b>thiazole hydrobromide

Guidance literature:: Multi-step reaction with 2 steps

1: 22 percent / K₂CO₃ / dimethylformamide / 3 h / Heating

2: 52 percent / BBr₃ / CH₂Cl₂ / Ambient temperature

With boron tribromide; potassium carbonate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00147a008