Technology Process of C35H38N2O11
There total 24 articles about C35H38N2O11 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
osmium(VIII) oxide; methanesulfonamide; quinuclidine hydrochloride; potassium hexacyanoferrate(III);
In
water; tert-butyl alcohol;
at 20 ℃;
for 39h;
DOI:10.1021/ja408034x
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: lithium hydroxide monohydrate; water / ethanol / 5 h / Reflux
2.1: tert.-butylnitrite; boron trifluoride diethyl etherate / tetrahydrofuran / 1 h / -15 - 0 °C / Inert atmosphere
2.2: 1 h / 0 - 20 °C
3.1: quinuclidine hydrochloride; methanesulfonamide; potassium hexacyanoferrate(III); osmium(VIII) oxide / water; tert-butyl alcohol / 39 h / 20 °C
With
osmium(VIII) oxide; tert.-butylnitrite; lithium hydroxide monohydrate; methanesulfonamide; boron trifluoride diethyl etherate; water; quinuclidine hydrochloride; potassium hexacyanoferrate(III);
In
tetrahydrofuran; ethanol; water; tert-butyl alcohol;
DOI:10.1021/ja408034x
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: tert.-butylnitrite; boron trifluoride diethyl etherate / tetrahydrofuran / 1 h / -15 - 0 °C / Inert atmosphere
1.2: 1 h / 0 - 20 °C
2.1: quinuclidine hydrochloride; methanesulfonamide; potassium hexacyanoferrate(III); osmium(VIII) oxide / water; tert-butyl alcohol / 39 h / 20 °C
With
osmium(VIII) oxide; tert.-butylnitrite; methanesulfonamide; boron trifluoride diethyl etherate; quinuclidine hydrochloride; potassium hexacyanoferrate(III);
In
tetrahydrofuran; water; tert-butyl alcohol;
DOI:10.1021/ja408034x
