(2S,3S)-3--2-hydroxy-4-phenyl-1-(N-prolylisoleucylvaline methyl ester)butane

Base Information

Chemical Name:(2S,3S)-3--2-hydroxy-4-phenyl-1-(N-prolylisoleucylvaline methyl ester)butane
CAS No.:132259-52-0
Molecular Formula:C₃₂H₅₂N₄O₇
Molecular Weight:604.787
Hs Code.:

(2S,3S)-3-<N-(tert-butoxycarbonyl)amino>-2-hydroxy-4-phenyl-1-(N-prolylisoleucylvaline methyl ester)butane

Synonyms:(2S,3S)-3--2-hydroxy-4-phenyl-1-(N-prolylisoleucylvaline methyl ester)butane

Suppliers and Price of (2S,3S)-3--2-hydroxy-4-phenyl-1-(N-prolylisoleucylvaline methyl ester)butane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3S)-3--2-hydroxy-4-phenyl-1-(N-prolylisoleucylvaline methyl ester)butane

Chemical Property:

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Technology Process of (2S,3S)-3--2-hydroxy-4-phenyl-1-(N-prolylisoleucylvaline methyl ester)butane

There total 2 articles about (2S,3S)-3--2-hydroxy-4-phenyl-1-(N-prolylisoleucylvaline methyl ester)butane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 132234-31-2
prolylisoleucyclvaline methyl ester hydrochloride

: 98760-08-8
(2R,3S)-3-[N-(tert-butyloxycarbonyl)amino]-1,2-epoxy-4-phenylbutane

: 132259-52-0
(2S,3S)-3--2-hydroxy-4-phenyl-1-(N-prolylisoleucylvaline methyl ester)butane

Guidance literature:: With triethylamine; In methanol; Heating;
DOI:10.1021/jm00107a049

Reference yield:

: 103127-52-2,107202-43-7
((S)-1-benzylallyl)carbamic acid tert-butyl ester

: 132259-52-0
(2S,3S)-3--2-hydroxy-4-phenyl-1-(N-prolylisoleucylvaline methyl ester)butane

Guidance literature:: Multi-step reaction with 2 steps

1: mCPBA / CH₂Cl₂ / 0 °C

2: triethylamine / diisopropyl ether / 24 h / Heating

With triethylamine; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; di-isopropyl ether;
DOI:10.1021/jm00099a008