4b,9b-dihydroxy-5-phenyl-4b,5,6,7,8,9b-hexahydroindeno[1,2-b]indole-9,10-dione

Base Information

• Chemical Name: 4b,9b-dihydroxy-5-phenyl-4b,5,6,7,8,9b-hexahydroindeno[1,2-b]indole-9,10-dione
• CAS No.: 1158819-85-2
• Molecular Formula: C₂₁H₁₇NO₄
• Molecular Weight: 347.37
• Mol file: 1158819-85-2.mol

Synonyms:4b,9b-dihydroxy-5-phenyl-4b,5,6,7,8,9b-hexahydroindeno[1,2-b]indole-9,10-dione

Chemical Property of 4b,9b-dihydroxy-5-phenyl-4b,5,6,7,8,9b-hexahydroindeno[1,2-b]indole-9,10-dione

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4b,9b-dihydroxy-5-phenyl-4b,5,6,7,8,9b-hexahydroindeno[1,2-b]indole-9,10-dione

There total 3 articles about 4b,9b-dihydroxy-5-phenyl-4b,5,6,7,8,9b-hexahydroindeno[1,2-b]indole-9,10-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

indan-1,2,3-trione hydrate (485-47-2) + 1,3-cylohexanedione (504-02-9) + aniline (62-53-3) → 4b,9b-dihydroxy-5-phenyl-4b,5,6,7,8,9b-hexahydroindeno[1,2-b]indole-9,10-dione (1158819-85-2)

Guidance literature:

With Fe₃O₄ magnetic nanoparticles in the layers of montmorillonite; In water; at 70 ℃; for 0.5h; Green chemistry;

DOI:10.1007/s11164-018-3659-7

Reference yield: 91.0%

indan-1,2,3-trione hydrate (485-47-2) + 3-phenylaminocyclohex-2-enone (24706-50-1) → 4b,9b-dihydroxy-5-phenyl-4b,5,6,7,8,9b-hexahydroindeno[1,2-b]indole-9,10-dione (1158819-85-2)

Guidance literature:

at 20 ℃;

DOI:10.1055/s-0028-1087983

Reference yield: 90.0%

indantrione (938-24-9) + 1,3-cylohexanedione (504-02-9) + aniline (62-53-3) → 4b,9b-dihydroxy-5-phenyl-4b,5,6,7,8,9b-hexahydroindeno[1,2-b]indole-9,10-dione (1158819-85-2)

Guidance literature:

1,3-cylohexanedione; aniline; With tin oxide; In water; at 70 ℃; for 0.5h; Green chemistry;

indantrione; In water; for 2h; Green chemistry;

DOI:10.1039/c4ra12618a

upstream raw materials:

indan-1,2,3-trione hydrate

3-phenylaminocyclohex-2-enone

indantrione

1,3-cylohexanedione

Downstream raw materials:

5-phenyl-5,6,7,8-tetrahydroindeno[1,2-b]indole-9,10-dione