4,5-diphenyl-2-<<5-<<2(2-hydroxyethoxy)ethyl>amino>pentyl>thio>-1H-imidazole

Base Information

Chemical Name:4,5-diphenyl-2-<<5-<<2(2-hydroxyethoxy)ethyl>amino>pentyl>thio>-1H-imidazole
CAS No.:162688-08-6
Molecular Formula:C₂₄H₃₁N₃O₂S
Molecular Weight:425.595
Hs Code.:

Synonyms:4,5-diphenyl-2-<<5-<<2(2-hydroxyethoxy)ethyl>amino>pentyl>thio>-1H-imidazole

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Chemical Property of 4,5-diphenyl-2-<<5-<<2(2-hydroxyethoxy)ethyl>amino>pentyl>thio>-1H-imidazole

Chemical Property:

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Technology Process of 4,5-diphenyl-2-<<5-<<2(2-hydroxyethoxy)ethyl>amino>pentyl>thio>-1H-imidazole

There total 5 articles about 4,5-diphenyl-2-<<5-<<2(2-hydroxyethoxy)ethyl>amino>pentyl>thio>-1H-imidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 162688-07-5
N-<2-(2-hydroxyethoxy)ethyl>-5-<(4,5-diphenyl-1H-imidazol-2-yl)thio>pentanamide

: 162688-08-6
4,5-diphenyl-2-<<5-<<2(2-hydroxyethoxy)ethyl>amino>pentyl>thio>-1H-imidazole

Guidance literature:: With sodium bis(2-methoxyethoxy)aluminium dihydride; In toluene; for 4h; Yield given; Heating;
DOI:10.1021/jm00007a004

Reference yield:

: 4509-90-4
5-bromovaleroyl chloride

: 162688-08-6
4,5-diphenyl-2-<<5-<<2(2-hydroxyethoxy)ethyl>amino>pentyl>thio>-1H-imidazole

Guidance literature:: Multi-step reaction with 3 steps

1: 32 percent / Et₃N / tetrahydrofuran / 48 h

2: 96 percent / K₂CO₃, tetra-n-butylammonium iodide / tetrahydrofuran / 2 h / Heating

3: sodium bis(2-methoxyethoxy)aluminum hydride / toluene / 4 h / Heating

With tetra-(n-butyl)ammonium iodide; potassium carbonate; triethylamine; sodium bis(2-methoxyethoxy)aluminium dihydride; In tetrahydrofuran; toluene;
DOI:10.1021/jm00007a004

Reference yield:

: 119-53-9,579-44-2
2-hydroxy-2-phenylacetophenone

: 162688-08-6
4,5-diphenyl-2-<<5-<<2(2-hydroxyethoxy)ethyl>amino>pentyl>thio>-1H-imidazole

Guidance literature:: Multi-step reaction with 3 steps

1: dimethylformamide; various solvent(s) / 160 °C

2: 96 percent / K₂CO₃, tetra-n-butylammonium iodide / tetrahydrofuran / 2 h / Heating

3: sodium bis(2-methoxyethoxy)aluminum hydride / toluene / 4 h / Heating

With tetra-(n-butyl)ammonium iodide; potassium carbonate; sodium bis(2-methoxyethoxy)aluminium dihydride; In tetrahydrofuran; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jm00007a004