3-Methyl-but-2-enoic acid 4-hydroxy-2,6-diiodo-3-(3-methyl-but-2-enoyl)-phenyl ester

Base Information

Chemical Name:3-Methyl-but-2-enoic acid 4-hydroxy-2,6-diiodo-3-(3-methyl-but-2-enoyl)-phenyl ester
CAS No.:84945-25-5
Molecular Formula:C₁₆H₁₆I₂O₄
Molecular Weight:526.11
Hs Code.:

Synonyms:3-Methyl-but-2-enoic acid 4-hydroxy-2,6-diiodo-3-(3-methyl-but-2-enoyl)-phenyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-Methyl-but-2-enoic acid 4-hydroxy-2,6-diiodo-3-(3-methyl-but-2-enoyl)-phenyl ester

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Technology Process of 3-Methyl-but-2-enoic acid 4-hydroxy-2,6-diiodo-3-(3-methyl-but-2-enoyl)-phenyl ester

There total 2 articles about 3-Methyl-but-2-enoic acid 4-hydroxy-2,6-diiodo-3-(3-methyl-but-2-enoyl)-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 84945-24-4
2',6'-diiodohydroquinone bis(3,3-dimethylacrylate)

: 84945-25-5
3-Methyl-but-2-enoic acid 4-hydroxy-2,6-diiodo-3-(3-methyl-but-2-enoyl)-phenyl ester

Guidance literature:: With sulfuric acid; In benzene; for 3h; Ambient temperature;
DOI:10.1021/ja00347a040

Reference yield:

: 1955-21-1
2,6-diiodohydroquinone

: 84945-25-5
3-Methyl-but-2-enoic acid 4-hydroxy-2,6-diiodo-3-(3-methyl-but-2-enoyl)-phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / triethylamine / diethyl ether / 2.5 h / Ambient temperature

2: conc. sulfuric acid / benzene / 3 h / Ambient temperature

With sulfuric acid; triethylamine; In diethyl ether; benzene;
DOI:10.1021/ja00347a040