C₂₄H₂₁F₃N₂O₂

Base Information

Chemical Name:C₂₄H₂₁F₃N₂O₂
CAS No.:1188489-61-3
Molecular Formula:C₂₄H₂₁F₃N₂O₂
Molecular Weight:426.438
Hs Code.:

C<sub>24</sub>H<sub>21</sub>F<sub>3</sub>N<sub>2</sub>O<sub>2</sub>

Synonyms:C₂₄H₂₁F₃N₂O₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₄H₂₁F₃N₂O₂

Chemical Property:

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Technology Process of C₂₄H₂₁F₃N₂O₂

There total 9 articles about C₂₄H₂₁F₃N₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 1188489-34-0
C₂₅H₂₃F₃N₂O₂

: 1188489-61-3
C₂₄H₂₁F₃N₂O₂

Guidance literature:: With hydrogenchloride; water; In 1,4-dioxane; at 80 ℃;

Reference yield:

: 670-80-4
4-cyclohexen-1-ylmorpholine

: 1188489-61-3
C₂₄H₂₁F₃N₂O₂

Guidance literature:: Multi-step reaction with 9 steps

1.1: dichloromethane / 20 °C

2.1: sulfuric acid / 0.5 h / 100 °C

3.1: sulfuric acid / 0.25 h / 100 °C

4.1: trichlorophosphate / Reflux

5.1: methanol / 20 °C / Reflux

6.1: bis-triphenylphosphine-palladium(II) chloride / toluene / 18 h / 80 °C / Inert atmosphere

7.1: potassium tert-butylate / methanol; dimethyl sulfoxide / 10 °C / Inert atmosphere

7.2: 1.25 h / 10 °C

8.1: potassium tert-butylate / tetrahydrofuran / 10 - 20 °C / Inert atmosphere

9.1: hydrogenchloride; water / 1,4-dioxane / 80 °C

With hydrogenchloride; sulfuric acid; potassium tert-butylate; water; trichlorophosphate; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; dimethyl sulfoxide; toluene;

Reference yield:

: 1188489-22-6
C₁₃H₁₄BrNO₂

: 1188489-61-3
C₂₄H₂₁F₃N₂O₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: sulfuric acid / 0.25 h / 100 °C

2.1: trichlorophosphate / Reflux

3.1: methanol / 20 °C / Reflux

4.1: bis-triphenylphosphine-palladium(II) chloride / toluene / 18 h / 80 °C / Inert atmosphere

5.1: potassium tert-butylate / methanol; dimethyl sulfoxide / 10 °C / Inert atmosphere

5.2: 1.25 h / 10 °C

6.1: potassium tert-butylate / tetrahydrofuran / 10 - 20 °C / Inert atmosphere

7.1: hydrogenchloride; water / 1,4-dioxane / 80 °C

With hydrogenchloride; sulfuric acid; potassium tert-butylate; water; trichlorophosphate; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; 1,4-dioxane; methanol; dimethyl sulfoxide; toluene;